1-(氯甲基)-4-十二烷基苯

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: The procedure of Example 1 is repeated using 16.0 g of sodium carbonate, 2.57 g of hydroxylamine hydrochloride and 21.83 g of p-dodecylbenzyl chloride in 75 ml of dimethylformamide kept at 50°-55° C. overnight under nitrogen. The product is isolated as a light brown oil. The product is isolated as a light brown oil

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: The procedure of Example 1 is repeated using 16.0 g of sodium carbonate, 2.57 g of hydroxylamine hydrochloride and 21.83 g of p-dodecylbenzyl chloride in 75 ml of dimethylformamide kept at 50°-55° C. overnight under nitrogen. The product is isolated as a light brown oil. The product is isolated as a light brown oil

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: The procedure of Example 1 is repeated using 16.0 g of sodium carbonate, 2.57 g of hydroxylamine hydrochloride and 21.83 g of p-dodecylbenzyl chloride in 75 ml of dimethylformamide kept at 50°-55° C. overnight under nitrogen. The product is isolated as a light brown oil. The product is isolated as a light brown oil

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: The procedure of Example 1 is repeated using 16.0 g of sodium carbonate, 2.57 g of hydroxylamine hydrochloride and 21.83 g of p-dodecylbenzyl chloride in 75 ml of dimethylformamide kept at 50°-55° C. overnight under nitrogen. The product is isolated as a light brown oil. The product is isolated as a light brown oil