2-(2-丙氧基苯基)乙醇

反应条件: temp:60.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A mixture of 2-hydroxyphenethyl alcohol (1.5 g), 1-bromopropane (1.3 ml), potassium carbonate (2.25 g) and acetone (50 ml) was stirred at 60° C. for 64 hours. After concentration under reduced pressure, the residue was mixed with water and was extracted with ethyl acetate. The organic layer was washed with a 1 N aqueous solution of sodium hydroxide and an aqueous saturated solution of sodium chloride, and was dried with magnesium sulfate. The resulting organic layer was concentrated under reduced pressure to obtain 2-propoxyphenethyl alcohol (2.02 g) as a yellow oily substance. After concentration under reduced pressure the residue was mixed with water was extracted with ethyl acetate The organic layer was washed with a 1 N aqueous solution of sodium hydroxide an aqueous saturated solution of sodium chloride, and was dried with magnesium sulfate The resulting organic layer was concentrated under reduced pressure