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CCOC(=O)C1CNCCO1产品信息
吗啉-2-羧酸乙酯（CAS 107904-06-3）的产品身份、结构标识及相关反应资料，供化学中间体检索、研发和采购评估使用。
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合成路线数据
8 条反应 · 8 篇文献
反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-8d42ce2c14664a76b3058cd82de27d5b反应条件: temp:100.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: A mixture of ethyl morpholine-2-carboxylate (3 g, 18.85 mmol) and ethyl acrylate (5 ml, 18.85 mmol) was heated at 100° C. for 14 h. The reaction was cooled to RT then diluted with Et2O and extracted with aqueous 3M HCl. The combined aqueous layers were basified by solid K2CO3 and extracted with DCM. The combined organic layers were dried over anhydrous Na2SO4, filtered and concentrated under reduced pressure to afford the title compound as a pale-yellow oil, which was used without further purification. The reaction was cooled to RT extracted with aqueous 3M HCl extracted with DCM The combined organic layers were dried over anhydrous Na2SO4 filtered concentrated under reduced pressure
来源 ID: ord-3ddb97006a7d4eeab694b2a3cd377a73反应条件: temp:100.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: A mixture of ethyl morpholine-2-carboxylate (3 g, 18.85 mmol) and ethyl acrylate (5 ml, 18.85 mmol) was heated at 100° C. for 14 h. The reaction was cooled to RT then diluted with Et2O and extracted with aqueous 3M HCl. The combined aqueous layers were basified by solid K2CO3 and extracted with DCM. The combined organic layers were dried over anhydrous Na2SO4, filtered and concentrated under reduced pressure to afford the title compound as a pale-yellow oil, which was used without further purification. The reaction was cooled to RT extracted with aqueous 3M HCl extracted with DCM The combined organic layers were dried over anhydrous Na2SO4 filtered concentrated under reduced pressure
来源 ID: ord-3ddb97006a7d4eeab694b2a3cd377a73反应条件: temp:100.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: A mixture of ethyl morpholine-2-carboxylate (3 g, 18.85 mmol) and ethyl acrylate (5 ml, 18.85 mmol) was heated at 100° C. for 14 h. The reaction was cooled to RT then diluted with Et2O and extracted with aqueous 3M HCl. The combined aqueous layers were basified by solid K2CO3 and extracted with DCM. The combined organic layers were dried over anhydrous Na2SO4, filtered and concentrated under reduced pressure to afford the title compound as a pale-yellow oil, which was used without further purification. The reaction was cooled to RT extracted with aqueous 3M HCl extracted with DCM The combined organic layers were dried over anhydrous Na2SO4 filtered concentrated under reduced pressure
来源 ID: ord-269a8acf6abe4520bcb17149a8afaff3反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-8d42ce2c14664a76b3058cd82de27d5b反应条件: temp:100.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: A mixture of ethyl morpholine-2-carboxylate (3 g, 18.85 mmol) and ethyl acrylate (5 ml, 18.85 mmol) was heated at 100° C. for 14 h. The reaction was cooled to RT then diluted with Et2O and extracted with aqueous 3M HCl. The combined aqueous layers were basified by solid K2CO3 and extracted with DCM. The combined organic layers were dried over anhydrous Na2SO4, filtered and concentrated under reduced pressure to afford the title compound as a pale-yellow oil, which was used without further purification. The reaction was cooled to RT extracted with aqueous 3M HCl extracted with DCM The combined organic layers were dried over anhydrous Na2SO4 filtered concentrated under reduced pressure
来源 ID: ord-33ad05b0ab804b288b8aa1dd0e10474b反应条件: temp:100.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: A mixture of ethyl morpholine-2-carboxylate (3 g, 18.85 mmol) and ethyl acrylate (5 ml, 18.85 mmol) was heated at 100° C. for 14 h. The reaction was cooled to RT then diluted with Et2O and extracted with aqueous 3M HCl. The combined aqueous layers were basified by solid K2CO3 and extracted with DCM. The combined organic layers were dried over anhydrous Na2SO4, filtered and concentrated under reduced pressure to afford the title compound as a pale-yellow oil, which was used without further purification. The reaction was cooled to RT extracted with aqueous 3M HCl extracted with DCM The combined organic layers were dried over anhydrous Na2SO4 filtered concentrated under reduced pressure
来源 ID: ord-3ddb97006a7d4eeab694b2a3cd377a73反应条件: temp:100.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: A mixture of ethyl morpholine-2-carboxylate (3 g, 18.85 mmol) and ethyl acrylate (5 ml, 18.85 mmol) was heated at 100° C. for 14 h. The reaction was cooled to RT then diluted with Et2O and extracted with aqueous 3M HCl. The combined aqueous layers were basified by solid K2CO3 and extracted with DCM. The combined organic layers were dried over anhydrous Na2SO4, filtered and concentrated under reduced pressure to afford the title compound as a pale-yellow oil, which was used without further purification. The reaction was cooled to RT extracted with aqueous 3M HCl extracted with DCM The combined organic layers were dried over anhydrous Na2SO4 filtered concentrated under reduced pressure
来源 ID: ord-269a8acf6abe4520bcb17149a8afaff3PubChem References
以下资料来自该化合物的公开数据库参考记录。
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