01
反应 #4061156
反应式
暂无可渲染的结构数据
暂无可渲染的结构数据
暂无可渲染的结构数据
相关文献 (1)
openreactiondata ↗doi:10.1039/C8SC04228D
反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-7ea697133d584bf7b18add82bb347dde2D 化学结构数据库编号 13176811
暂无可渲染的结构数据
SMILES
CC(CC1=CC(=C(C=C1)OC)S(=O)(=O)N)N——
产品信息
5-(2-氨基丙基)-2-甲氧基苯磺酰胺
5-(2-氨基丙基)-2-甲氧基苯磺酰胺（CAS 112244-38-9）的产品身份、结构标识及相关反应资料，供化学中间体检索、研发和采购评估使用。
CAS号112244-38-9
数据库编号13176811
分子式—
更新时间2023-01-08
可能的应用方向
可能的应用方向
仅供专业研发与工业用途
数据库编号 13176811
计算性质
精确质量—
XLogP—
拓扑极性表面积—
氢键供体数—
氢键受体数—
可旋转键数—
- IUPAC 名称
- —
- InChIKey
- —
- SMILES
- CC(CC1=CC(=C(C=C1)OC)S(=O)(=O)N)N
- InChI
- —
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安全与说明
仅供专业研发与工业用途。操作前请依据供应商提供的安全数据表完成风险评估。
合成路线数据
相关反应
10 条反应 · 10 篇文献
02
反应 #3856381
反应式
暂无可渲染的结构数据
+暂无可渲染的结构数据
+暂无可渲染的结构数据
›
暂无可渲染的结构数据
相关文献 (1)
openreactiondata ↗doi:10.1039/C8SC04228D
反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-cc09ff2777d546f6a0999ea6acc6768e03
反应 #3463102
反应式
暂无可渲染的结构数据
+暂无可渲染的结构数据
›
暂无可渲染的结构数据
相关文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US06965051B2
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 5-(−2-aminopropyl]-2-methoxybenzenesulfonamide (200 g) was dissolved in dimethylformamide (950 ml) and 1-(2-Bromoethoxy)-2-ethoxybenzene (100.3 g) was added. The reaction mixture was heated to 80–85° C. for 4 hours. Dimethylformamide was then distilled off under vacuum. Water (1000 ml) was added to solid residue and the mixture was heated to 80–90° C. under stirring for 2 hours. The mixture was cooled to room temperature. Formed crystals were filtered off and were suspended in water (900 ml). Suspension was heated to 80–90° C. under stirring for 2 hours. Crystals were filtered, washed with water (200 ml) and dried to give tamsulosin base (150 g, 89.8%). The reaction mixture was heated to 80–85° C. for 4 hours Dimethylformamide was then distilled off under vacuum Water (1000 ml) was added to solid residue the mixture was heated to 80–90° C. Formed crystals were filtered off Suspension was heated to 80–90° C. under stirring for 2 hours Crystals were filtered washed with water (200 ml) dried
来源 ID: ord-ae2a2355a73d4a43a76916fc8e19fdc404
反应 #3463101
反应式
暂无可渲染的结构数据
+暂无可渲染的结构数据
›
暂无可渲染的结构数据
相关文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US06965051B2
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 5-(−2-aminopropyl]-2-methoxybenzenesulfonamide (200 g) was dissolved in dimethylformamide (950 ml) and 1-(2-Bromoethoxy)-2-ethoxybenzene (100.3 g) was added. The reaction mixture was heated to 80–85° C. for 4 hours. Dimethylformamide was then distilled off under vacuum. Water (1000 ml) was added to solid residue and the mixture was heated to 80–90° C. under stirring for 2 hours. The mixture was cooled to room temperature. Formed crystals were filtered off and were suspended in water (900 ml). Suspension was heated to 80–90° C. under stirring for 2 hours. Crystals were filtered, washed with water (200 ml) and dried to give tamsulosin base (150 g, 89.8%). The reaction mixture was heated to 80–85° C. for 4 hours Dimethylformamide was then distilled off under vacuum Water (1000 ml) was added to solid residue the mixture was heated to 80–90° C. Formed crystals were filtered off Suspension was heated to 80–90° C. under stirring for 2 hours Crystals were filtered washed with water (200 ml) dried
来源 ID: ord-ae2a2355a73d4a43a76916fc8e19fdc405
反应 #2429569
反应式
暂无可渲染的结构数据
+暂无可渲染的结构数据
›
暂无可渲染的结构数据
相关文献 (1)
openreactiondata ↗doi:10.1039/C8SC04228D
反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-7ea697133d584bf7b18add82bb347dde06
反应 #2264334
反应式
暂无可渲染的结构数据
+暂无可渲染的结构数据
+暂无可渲染的结构数据
›
暂无可渲染的结构数据
相关文献 (1)
openreactiondata ↗doi:10.1039/C8SC04228D
反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-cc09ff2777d546f6a0999ea6acc6768e07
反应 #2100059
反应式
暂无可渲染的结构数据
+暂无可渲染的结构数据
›
暂无可渲染的结构数据
相关文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US06835853B2
反应条件: temp:82.51; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 5-(-2-aminopropyl]-2-methoxybenzenesulfonamide (200 g) was dissolved in dimethylformamide (950 ml) and 1-(2-Bromoethoxy)-2-ethoxybenzene (100.3 g) was added. The reaction mixture was heated to 80-85° C. for 4 hours. Dimethylformamide was then distilled off under vacuum. Water (1000 ml) was added to solid residue and the mixture was heated to 80-90° C. under stirring for 2 hours. The mixture was cooled to room temperature. Formed crystals were filtered off and were suspended in water (900 ml). Suspension was heated to 80-90° C. under stirring for 2 hours. Crystals were filtered, washed with water (200 ml) and dried to give tamsulosin base (150 g, 89.8%). Dimethylformamide was then distilled off under vacuum Water (1000 ml) was added to solid residue the mixture was heated to 80-90° C. The mixture was cooled to room temperature Formed crystals were filtered off Suspension was heated to 80-90° C. under stirring for 2 hours Crystals were filtered washed with water (200 ml) dried
来源 ID: ord-bf6f2e98215b4b97ab98e26369938b7c08
反应 #2100060
反应式
暂无可渲染的结构数据
+暂无可渲染的结构数据
›
暂无可渲染的结构数据
相关文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US06835853B2
反应条件: temp:82.51; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 5-(-2-aminopropyl]-2-methoxybenzenesulfonamide (200 g) was dissolved in dimethylformamide (950 ml) and 1-(2-Bromoethoxy)-2-ethoxybenzene (100.3 g) was added. The reaction mixture was heated to 80-85° C. for 4 hours. Dimethylformamide was then distilled off under vacuum. Water (1000 ml) was added to solid residue and the mixture was heated to 80-90° C. under stirring for 2 hours. The mixture was cooled to room temperature. Formed crystals were filtered off and were suspended in water (900 ml). Suspension was heated to 80-90° C. under stirring for 2 hours. Crystals were filtered, washed with water (200 ml) and dried to give tamsulosin base (150 g, 89.8%). Dimethylformamide was then distilled off under vacuum Water (1000 ml) was added to solid residue the mixture was heated to 80-90° C. The mixture was cooled to room temperature Formed crystals were filtered off Suspension was heated to 80-90° C. under stirring for 2 hours Crystals were filtered washed with water (200 ml) dried
来源 ID: ord-bf6f2e98215b4b97ab98e26369938b7c09
反应 #2100058
反应式
暂无可渲染的结构数据
+暂无可渲染的结构数据
›
暂无可渲染的结构数据
相关文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US06835853B2
反应条件: temp:82.51; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 5-(-2-aminopropyl]-2-methoxybenzenesulfonamide (200 g) was dissolved in dimethylformamide (950 ml) and 1-(2-Bromoethoxy)-2-ethoxybenzene (100.3 g) was added. The reaction mixture was heated to 80-85° C. for 4 hours. Dimethylformamide was then distilled off under vacuum. Water (1000 ml) was added to solid residue and the mixture was heated to 80-90° C. under stirring for 2 hours. The mixture was cooled to room temperature. Formed crystals were filtered off and were suspended in water (900 ml). Suspension was heated to 80-90° C. under stirring for 2 hours. Crystals were filtered, washed with water (200 ml) and dried to give tamsulosin base (150 g, 89.8%). Dimethylformamide was then distilled off under vacuum Water (1000 ml) was added to solid residue the mixture was heated to 80-90° C. The mixture was cooled to room temperature Formed crystals were filtered off Suspension was heated to 80-90° C. under stirring for 2 hours Crystals were filtered washed with water (200 ml) dried
来源 ID: ord-bf6f2e98215b4b97ab98e26369938b7c10
反应 #948040
反应式
暂无可渲染的结构数据
+暂无可渲染的结构数据
›
暂无可渲染的结构数据
相关文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US06965051B2
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 5-(−2-aminopropyl]-2-methoxybenzenesulfonamide (200 g) was dissolved in dimethylformamide (950 ml) and 1-(2-Bromoethoxy)-2-ethoxybenzene (100.3 g) was added. The reaction mixture was heated to 80–85° C. for 4 hours. Dimethylformamide was then distilled off under vacuum. Water (1000 ml) was added to solid residue and the mixture was heated to 80–90° C. under stirring for 2 hours. The mixture was cooled to room temperature. Formed crystals were filtered off and were suspended in water (900 ml). Suspension was heated to 80–90° C. under stirring for 2 hours. Crystals were filtered, washed with water (200 ml) and dried to give tamsulosin base (150 g, 89.8%). The reaction mixture was heated to 80–85° C. for 4 hours Dimethylformamide was then distilled off under vacuum Water (1000 ml) was added to solid residue the mixture was heated to 80–90° C. Formed crystals were filtered off Suspension was heated to 80–90° C. under stirring for 2 hours Crystals were filtered washed with water (200 ml) dried
来源 ID: ord-ae2a2355a73d4a43a76916fc8e19fdc4PubChem References
公开参考资料
以下资料来自该化合物的公开数据库参考记录。
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