反应 #3250349
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openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US08969568B2
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 100 mg Methyl 2-(5-oxopyrrolidine-3-yl)acetate (I.26) was placed in tetrahydrofuran and 30 mg lithium borohydride was added and the mixture stirred at ambient temperature overnight. The suspension was diluted with saturated sodium chloride solution and extracted with ethyl acetate (×3). The water phase was freeze dried. extracted with ethyl acetate (×3) dried
来源 ID: ord-e0c924d9d353432798a696a1092701aa