反应 #4124967
相关文献 (1)
openreactiondata ↗doi:10.1039/C8SC04228D
反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-9098c3aa3b7e4a7c81e69d45553b94e8暂无可渲染的结构数据
C1=CC=C2C(=C1)C=C(O2)S(=O)(=O)N产品信息
1-苯并呋喃-2-磺酰胺(CAS 124043-72-7)的产品身份、结构标识及相关反应资料,供化学中间体检索、研发和采购评估使用。
可能的应用方向
仅供专业研发与工业用途
数据库编号 10750432
安全提示
仅供专业研发与工业用途。操作前请依据供应商提供的安全数据表完成风险评估。
合成路线数据
12 条反应 · 12 篇文献
反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-9098c3aa3b7e4a7c81e69d45553b94e8反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 2-Benzofuransulfonamide (7.6 mmol), prepared as described in Preparation 2, was reacted with 3,4-dichlorophenylisocyanate (7.6 mmol) as described in Preparation 2 to obtain 2.4 g of the title product as a solid. as described in Preparation 2 as described in Preparation 2
来源 ID: ord-db7f84a67980438fbf9dc52f94c0ae28反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 2-Benzofuransulfonamide (7.6 mmol), prepared as described in Preparation 2, was reacted with 4-methylphenylisocyanate (7.6 mmol) as described in Preparation 2 to obtain 1.6 g of the title product as a solid. as described in Preparation 2 as described in Preparation 2
来源 ID: ord-46a5b4abb87d48ecbf829cc3c05b8fa7反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 2-Benzofuransulfonamide (7.6 mmol), prepared as described in Example 2, was reacted with 3,4-dichlorophenylisocyanate (7.6 mmol) as described in Example 2 to obtain 2.4 g of the title product as a solid.
来源 ID: ord-6f561fa3593e41e39b13a3a35f3a282d反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 2-Benzofuransulfonamide (7.6 mmol), prepared as described in Example 2, was reacted with 4-methylphenylisocyanate (7.6 mmol) as described in Example 2 to obtain 1.6 g of the title product as a solid.
来源 ID: ord-c44bdf14032d483e967b2f374071a1b6反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 2-Benzofuransulfonamide (7.6 mmol), prepared as described in Preparation 2, was reacted with 3,4-dichlorophenylisocyanate (7.6 mmol) as described in Preparation 2 to obtain 2.4 g of the title product as a solid. as described in Preparation 2 as described in Preparation 2
来源 ID: ord-db7f84a67980438fbf9dc52f94c0ae28反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 2-Benzofuransulfonamide (7.6 mmol), prepared as described in Preparation 2, was reacted with 3,4-dichlorophenylisocyanate (7.6 mmol) as described in Preparation 2 to obtain 2.4 g of the title product as a solid. as described in Preparation 2 as described in Preparation 2
来源 ID: ord-db7f84a67980438fbf9dc52f94c0ae28反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 2-Benzofuransulfonamide (7.6 mmol), prepared as described in Preparation 2, was reacted with 4-methylphenylisocyanate (7.6 mmol) as described in Preparation 2 to obtain 1.6 g of the title product as a solid. as described in Preparation 2 as described in Preparation 2
来源 ID: ord-46a5b4abb87d48ecbf829cc3c05b8fa7反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 2-Benzofuransulfonamide (7.6 mmol), prepared as described in Preparation 2, was reacted with 4-methylphenylisocyanate (7.6 mmol) as described in Preparation 2 to obtain 1.6 g of the title product as a solid. as described in Preparation 2 as described in Preparation 2
来源 ID: ord-46a5b4abb87d48ecbf829cc3c05b8fa7反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-9098c3aa3b7e4a7c81e69d45553b94e8反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 2-Benzofuransulfonamide (7.6 mmol), prepared as described in Example 1, was reacted with 4-bromophenylisocyanate (7.6 mmol) as described in Method A to obtain 2.3 g of the title product as a solid. 1H NMR (CD3SOCD3): δ9.35 (s, 1 H), 7.87 (d, J =8 Hz, 1 H), 7.82 (s, 1 H), 7.78 (d, J =8 Hz, 1 H), 7.58 (dd, J =8, 8 Hz, 1 H), 7.46 (d, J =9 Hz, 2 H), 7.44 (dd, J =8, 8 Hz, 1 H), 7.38 (d, J =9 Hz, 2 H).
来源 ID: ord-d9b68d4078014801878c21a74f7b5c8c反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 2-Benzofuransulfonamide (7.6 mmol), prepared as described in Example 1, was reacted with 3,4-dichlorophenylisocyanate (7.6 mmol) as described in Method A to obtain 2.4 g of the title product as a solid. 1H NMR (CD3SOCD3): δ9.43 (s, 1 H), 7.88 (d, J =8 Hz, 1 H), 7.85 (s, 1 H), 7.80 (m, 1 H), 7.76 (m, 1 H), 7.59 (dd, J =6, 8 Hz, 1 H), 7.52 (d, J =8 Hz, 1 H), 7.45 (dd, J =6, 8 Hz, 1 H), 7.35 (dd, J =3, 6 Hz, 1 H).
来源 ID: ord-df6526b6cffb4da7ae30accd3d4de07bPubChem References
以下资料来自该化合物的公开数据库参考记录。
