01
反应 #3869163
反应式
暂无可渲染的结构数据
暂无可渲染的结构数据
暂无可渲染的结构数据
暂无可渲染的结构数据
相关文献 (1)
openreactiondata ↗doi:10.1039/C8SC04228D
反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-ebab0ebe7e494f199fc50bcbf9b3742e2D 化学结构数据库编号 19794273
暂无可渲染的结构数据
SMILES
O(C(NCC1CC(C1)=O)=O)C(C)(C)C——
结构数据已核验 · 数据库编号 19794273
中间体产品
((3-氧代环丁基)甲基)氨基甲酸叔丁酯
Carbamic acid, [(3-oxocyclobutyl)methyl]-, 1,1-dimethylethyl ester (9CI)
CAS 130369-09-4Product ID 768911
✓
产品信息已核验
结构、标识符和计算性质已按 CAS 与数据库记录完成匹配。
| 中文名称 | ((3-氧代环丁基)甲基)氨基甲酸叔丁酯 |
|---|---|
| English name | Carbamic acid, [(3-oxocyclobutyl)methyl]-, 1,1-dimethylethyl ester (9CI) |
| IUPAC 名称 | — |
| CAS号 | 130369-09-4 |
| 数据库编号 | 19794273 |
| 分子式 | — |
| 分子量 | — |
产品信息
((3-氧代环丁基)甲基)氨基甲酸叔丁酯
((3-氧代环丁基)甲基)氨基甲酸叔丁酯（CAS 130369-09-4）的产品身份、结构标识及相关反应资料，供化学中间体检索、研发和采购评估使用。
CAS号130369-09-4
数据库编号19794273
分子式—
更新时间2025-04-09
可能的应用方向
可能的应用方向
仅供专业研发与工业用途
数据库编号 19794273
计算性质
精确质量—
XLogP—
拓扑极性表面积—
氢键供体数—
氢键受体数—
可旋转键数—
- IUPAC 名称
- —
- InChIKey
- —
- SMILES
- O(C(NCC1CC(C1)=O)=O)C(C)(C)C
- InChI
- —
安全提示
安全与说明
仅供专业研发与工业用途。操作前请依据供应商提供的安全数据表完成风险评估。
合成路线数据
相关反应
6 条反应 · 6 篇文献
02
反应 #2865068
反应式
暂无可渲染的结构数据
+暂无可渲染的结构数据
›
暂无可渲染的结构数据
相关文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US05153352
反应条件: temp:-78.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: In a round bottom flask were placed 9 g of the product from Step A of Example 9, 100 mL of methanol, and 400 mL of dichloromethane. The solution was cooled to -78° C., and ozone was bubbled through the reaction mixture until the solution was blue. The system was flushed with nitrogen for 2.5 h, and then treated with 34 mL of dimethylsulide. After 1 h at -78° C., 0° C. for 1 h, and room temperature for 1 h, the solution was stored in a refrigerator at 5° C. overnight before being concentrated. The crude material was purified by column chromatography to afford the title compound. In a round bottom flask were placed ozone was bubbled through the reaction mixture until the solution The system was flushed with nitrogen for 2.5 h treated with 34 mL of dimethylsulide 0° C. for 1 h room temperature for 1 h the solution was stored in a refrigerator at 5° C. overnight before being concentrated The crude material was purified by column chromatography
来源 ID: ord-b79984df2dc64b0698b8dd38c55c906d03
反应 #2521787
反应式
暂无可渲染的结构数据
+暂无可渲染的结构数据
›
暂无可渲染的结构数据
相关文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US05246931
反应条件: temp:-78.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: In a round bottom flask were placed 9 g of the product from Step A of Example 9, 100 mL of methanol, and 400 mL of dichloromethane. The solution was cooled to -78° C., and ozone was bubbled through the reaction mixture until the solution was blue. The system was flushed with nitrogen for 2.5 h, and then treated with 34 mL of dimethylsulide. After 1 h at -78° C., 0° C. for 1 h, and room temperature for 1 h, the solution was stored in a refrigerator at 5° C. overnight before being concentrated. The crude material was purified by column chromatography to afford the title compound. In a round bottom flask were placed ozone was bubbled through the reaction mixture until the solution The system was flushed with nitrogen for 2.5 h treated with 34 mL of dimethylsulide 0° C. for 1 h room temperature for 1 h the solution was stored in a refrigerator at 5° C. overnight before being concentrated The crude material was purified by column chromatography
来源 ID: ord-24eebc7913134719814d09f4259c412d04
反应 #2309194
反应式
暂无可渲染的结构数据
+暂无可渲染的结构数据
›
暂无可渲染的结构数据
相关文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US05246931
反应条件: temp:-78.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: In a round bottom flask were placed 9 g of the product from Step A of Example 9, 100 mL of methanol, and 400 mL of dichloromethane. The solution was cooled to -78° C., and ozone was bubbled through the reaction mixture until the solution was blue. The system was flushed with nitrogen for 2.5 h, and then treated with 34 mL of dimethylsulide. After 1 h at -78° C., 0° C. for 1 h, and room temperature for 1 h, the solution was stored in a refrigerator at 5° C. overnight before being concentrated. The crude material was purified by column chromatography to afford the title compound. In a round bottom flask were placed ozone was bubbled through the reaction mixture until the solution The system was flushed with nitrogen for 2.5 h treated with 34 mL of dimethylsulide 0° C. for 1 h room temperature for 1 h the solution was stored in a refrigerator at 5° C. overnight before being concentrated The crude material was purified by column chromatography
来源 ID: ord-24eebc7913134719814d09f4259c412d05
反应 #394710
反应式
暂无可渲染的结构数据
+暂无可渲染的结构数据
›
暂无可渲染的结构数据
相关文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US05153352
反应条件: temp:-78.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: In a round bottom flask were placed 9 g of the product from Step A of Example 9, 100 mL of methanol, and 400 mL of dichloromethane. The solution was cooled to -78° C., and ozone was bubbled through the reaction mixture until the solution was blue. The system was flushed with nitrogen for 2.5 h, and then treated with 34 mL of dimethylsulide. After 1 h at -78° C., 0° C. for 1 h, and room temperature for 1 h, the solution was stored in a refrigerator at 5° C. overnight before being concentrated. The crude material was purified by column chromatography to afford the title compound. In a round bottom flask were placed ozone was bubbled through the reaction mixture until the solution The system was flushed with nitrogen for 2.5 h treated with 34 mL of dimethylsulide 0° C. for 1 h room temperature for 1 h the solution was stored in a refrigerator at 5° C. overnight before being concentrated The crude material was purified by column chromatography
来源 ID: ord-b79984df2dc64b0698b8dd38c55c906d06
反应 #67778
反应式
暂无可渲染的结构数据
+暂无可渲染的结构数据
›
暂无可渲染的结构数据
相关文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US05246931
反应条件: temp:-78.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: In a round bottom flask were placed 9 g of the product from Step A of Example 9, 100 mL of methanol, and 400 mL of dichloromethane. The solution was cooled to -78° C., and ozone was bubbled through the reaction mixture until the solution was blue. The system was flushed with nitrogen for 2.5 h, and then treated with 34 mL of dimethylsulide. After 1 h at -78° C., 0° C. for 1 h, and room temperature for 1 h, the solution was stored in a refrigerator at 5° C. overnight before being concentrated. The crude material was purified by column chromatography to afford the title compound. In a round bottom flask were placed ozone was bubbled through the reaction mixture until the solution The system was flushed with nitrogen for 2.5 h treated with 34 mL of dimethylsulide 0° C. for 1 h room temperature for 1 h the solution was stored in a refrigerator at 5° C. overnight before being concentrated The crude material was purified by column chromatography
来源 ID: ord-24eebc7913134719814d09f4259c412dPubChem References
公开参考资料
以下资料来自该化合物的公开数据库参考记录。