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C1=CC=C(C=C1)CCNS(=O)(=O)C2=CC=C(C=C2)Cl产品信息
4-氯-N-(2-苯乙基)苯磺酰胺（CAS 133276-82-1）的产品身份、结构标识及相关反应资料，供化学中间体检索、研发和采购评估使用。
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7 条反应 · 7 篇文献
反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-cb8b1a6e63714d9e8f74d3bb9e2a1afa反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: To a mixture of 150 ml of ethylene chloride and 150 ml of water are added 30.3 g of 2-phenylethylamine, 12 g of sodium hydroxide and 0.5 g of tetrabutylammonium bromide. 65.5 g of 4-chlorobenzenesulphonic acid chloride are added to the mixture in batches with stirring. After 30 minutes the organic phase is separated off, evaporated down and the residue is recrystallised from toluene. After 30 minutes the organic phase is separated off evaporated down the residue is recrystallised from toluene
来源 ID: ord-4f4ffb16a9c7457da43b5a0b32bee11c反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: To a mixture of 150 ml of ethylene chloride and 150 ml of water are added 30.3 g of 2-phenylethylamine, 12 g of sodium hydroxide and 0.5 g of tetrabutylammonium bromide. 65.5 g of 4-chlorobenzenesulphonic acid chloride are added to the mixture in batches with stirring. After 30 minutes the organic phase is separated off, evaporated down and the residue is recrystallised from toluene. After 30 minutes the organic phase is separated off evaporated down the residue is recrystallised from toluene
来源 ID: ord-e2abf3686c71440cad7726de2d91b938反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: To a mixture of 150 ml of ethylene chloride and 150 ml of water are added 30.3 g of 2-phenylethylamine, 12 g of sodium hydroxide and 0.5 g of tetrabutylammonium bromide. 65.5 g of 4-chlorobenzenesulphonic acid chloride are added to the mixture in batches with stirring. After 30 minutes the organic phase is separated off, evaporated down and the residue is recrystallised from toluene. After 30 minutes the organic phase is separated off evaporated down the residue is recrystallised from toluene
来源 ID: ord-e2abf3686c71440cad7726de2d91b938反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: To a mixture of 150 ml of ethylene chloride and 150 ml of water are added 30.3 g of 2-phenylethylamine, 12 g of sodium hydroxide and 0.5 g of tetrabutylammonium bromide. 65.5 g of 4-chlorobenzenesulphonic acid chloride are added to the mixture in batches with stirring. After 30 minutes the organic phase is separated off, evaporated down and the residue is recrystallised from toluene. After 30 minutes the organic phase is separated off evaporated down the residue is recrystallised from toluene
来源 ID: ord-67782c2be1ce455088bebafa349fdd7c反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: To a mixture of 150 ml of ethylene chloride and 150 ml of water are added 30.3 g of 2-phenylethylamine, 12 g of sodium hydroxide and 0.5 g of tetrabutylammonium bromide. 65.5 g of 4-chlorobenzenesulphonic acid chloride are added to the mixture in batches with stirring. After 30 minutes the organic phase is separated off, evaporated down and the residue is recrystallised from toluene. After 30 minutes the organic phase is separated off evaporated down the residue is recrystallised from toluene
来源 ID: ord-4f4ffb16a9c7457da43b5a0b32bee11c反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: To a mixture of 150 ml of ethylene chloride and 150 ml of water are added 30.3 g of 2-phenylethylamine, 12 g of sodium hydroxide and 0.5 g of tetrabutylammonium bromide. 65.5 g of 4-chlorobenzenesulphonic acid chloride are added to the mixture in batches with stirring. After 30 minutes the organic phase is separated off, evaporated down and the residue is recrystallised from toluene. After 30 minutes the organic phase is separated off evaporated down the residue is recrystallised from toluene
来源 ID: ord-e2abf3686c71440cad7726de2d91b938PubChem References
以下资料来自该化合物的公开数据库参考记录。