反应 #1607317
相关文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US08946279B2
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: In a dried reaction flask, the crude (S)-butyl 3-(dimethylamino)pyrrolidine-1-carboxylate (2.0 g) obtained in the above step was added to CH2Cl2 (30 mL). HCl gas was passed thereto for 3 hr. The solution was concentrated under reduced pressure to obtain a crude yellow viscous material (1.6 g). In a dried reaction flask The solution was concentrated under reduced pressure
来源 ID: ord-b91bd3ab96414501a96e55d1fb2bf404