N-DECANOYLGLYCINE

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: N-Decanoylaminoperoxyacetic acid was prepared by reaction of N-decanoylglycine with hydrogen peroxide in methanesulfonic acid according to the procedure described in Example II. From 22.9 g (0.100 mol) of N-decanoylglycine and 17.0 g (0.500 mol) of hydrogen peroxide in 50 mL methanesulfonic acid was obtained 22.4 g of peroxyacid having an AvO of 6.06% (theoretical yield=24.5 g having an AvO of 6.53%), mp 75°-80° C. (melts with gas evolution).

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: N-Decanoylaminoperoxyacetic acid was prepared by reaction of N-decanoylglycine with hydrogen peroxide in methanesulfonic acid according to the procedure described in Example II. From 22.9 g (0.100 mol) of N-decanoylglycine and 17.0 g (0.500 mol) of hydrogen peroxide in 50 mL methanesulfonic acid was obtained 22.4 g of peroxyacid having an AvO of 6.06% (theoretical yield=24.5 g having an AvO of 6.53%), mp 75°-80° C. (melts with gas evolution).

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: N-Decanoylglycine was prepared by reaction of decanoyl chloride with glycine according to the procedure described in Example I. From 47.7 g (0.25 mol) of decanoyl chloride and 18.8 g (0.25 mol) of glycine was obtained 54.1 g (94%) of N-decanoylglycine, mp 104°-108° C.

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: N-Decanoylaminoperoxyacetic acid was prepared by reaction of N-decanoylglycine with hydrogen peroxide in methanesulfonic acid according to the procedure described in Example II. From 22.9 g (0.100 mol) of N-decanoylglycine and 17.0 g (0.500 mol) of hydrogen peroxide in 50 mL methanesulfonic acid was obtained 22.4 g of peroxyacid having an AvO of 6.06% (theoretical yield=24.5 g having an AvO of 6.53%), mp 75°-80° C. (melts with gas evolution).

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: N-Decanoylglycine was prepared by reaction of decanoyl chloride with glycine according to the procedure described in Example I. From 47.7 g (0.25 mol) of decanoyl chloride and 18.8 g (0.25 mol) of glycine was obtained 54.1 g (94%) of N-decanoylglycine, mp 104°-108° C.