3-甲基-4-苯基甲氧基苯胺

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: The procedure described in Example 1 was repeated using N′-[4-cyano-3-(2-hydroxyethoxy)-1H-pyrazol-5-yl]-N,N-dimethylimidoformamide (2.0 g, 8.96 mmol) and 3-methyl-4-benzyloxyaniline (2.1 g, 9.87 mmol) to give the title compound as a white solid (2.25 g, 64%); NMR Spectrum: 2.23 (s, 3H), 3.79 (t, 2H), 4.30 (t, 2H), 5.15 (s, 2H), 7.03 (d, 1H), 7.32-7.48 (m, 7H), 8.21 (s, 1H), 8.33 (s, 1H); Mass Spectrum: 392 (MH+).

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: The procedure described in Example 1 was repeated using N′-[4-cyano-3-(2-hydroxyethoxy)-1H-pyrazol-5-yl]-N,N-dimethylimidoformamide (2.0 g, 8.96 mmol) and 3-methyl-4-benzyloxyaniline (2.1 g, 9.87 mmol) to give the title compound as a white solid (2.25 g, 64%); NMR Spectrum: 2.23 (s, 3H), 3.79 (t, 2H), 4.30 (t, 2H), 5.15 (s, 2H), 7.03 (d, 1H), 7.32-7.48 (m, 7H), 8.21 (s, 1H), 8.33 (s, 1H); Mass Spectrum: 392 (MH+).

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: The procedure described in Example 1 was repeated using N′-[4-cyano-3-(2-hydroxyethoxy)-1H-pyrazol-5-yl]-N,N-dimethylimidoformamide (2.0 g, 8.96 mmol) and 3-methyl-4-benzyloxyaniline (2.1 g, 9.87 mmol) to give the title compound as a white solid (2.25 g, 64%); NMR Spectrum: 2.23 (s, 3H), 3.79 (t, 2H), 4.30 (t, 2H), 5.15 (s, 2H), 7.03 (d, 1H), 7.32-7.48 (m, 7H), 8.21 (s, 1H), 8.33 (s, 1H); Mass Spectrum: 392 (MH+).