反应 #1044556
相关文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US07115639B2
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: Following the general method as outlined in Example 59, starting from (2S,4EZ)-1-(tert-butoxycarbonyl)-4-(methoxyimino)-2-pyrrolidine-carboxylic acid (Intermediate 2), [1,1′-biphenyl]-4-carbonyl chloride, and 2-[(2-furylmethyl)sulfonyl]-N′-hydroxy-ethanimidamide, the title compound was obtained in 88% purity by HPLC. MS(ESI+): m/z=521.4.
来源 ID: ord-85ab661ab306486bbf8ba67526a1d917