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2,6-二氟苯甲酰胺（CAS 18063-03-1）的产品身份、结构标识及相关反应资料，供化学中间体检索、研发和采购评估使用。
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12 条反应 · 12 篇文献
反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-22723c72f6214e2bb4f23487f883a3a8反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-91bd2dcb7e9c41978ebf85cb0534de3e反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-0814d374c2744315a2629aa19a6c30fd反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-a1e79882963e4030acf48a9b1e2fa01f反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-34da9ab40afc4defa52b51dce0080d95反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-418ee23b62c94d3b96ccc0f07c1fc73b反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-53c3bd1e853349a3af8158ab448abdc0反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-a25c8570ec794cd7b1be074b6a358868反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-1383ca2304574c46a801477f8f8450ed反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: A mixture of 0.52 g of 2,6-difluorobenzamide and 0.33 ml of oxalyl chloride was stirred under reflux in 15 ml 1,2-dichloroethane overnight. Solvent was removed under vacuum and 10 ml 1,2-dichloroethane was added. Solvent was removed under vacuum to leave the title intermediate, which could be used directly or dissolved in 1,2-dichloroethane and stored for future use. Solvent was removed under vacuum and 10 ml 1,2-dichloroethane was added Solvent was removed under vacuum
来源 ID: ord-c3a3cc4554cc4285bc0b330a5ff92594反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: In order to synthesize the isocyanate, 1.57 g (10 mmol) of 2,6-difluorobenzamide and 15 ml of dry 1,2-dichloroethane were introduced into a 100 ml flask and then 0.92 g (10.5 mmol) of oxalyl chloride was slowly added thereto at normal temperature by means of a syringe, during which an exothermic reaction occurred that generated hydrochloride gas. The resulting reaction mixture was refluxed for 5 hours and cooled to normal temperature. The reaction solvent and the excess oxalyl chloride were removed therefrom under vacuo to obtain 2,6-difluorobenzoyl isocyanate in an oily state. Thus obtained 2,6-difluorobenzoyl isocyanate was then dissolved in 20 ml of dry 1,2-dichloroethane. Then, 2.63 g of 2-chloro-3,5-bis(trifluoromethyl)aniline was added thereto, reacted for 3 hours, and filtered to obtain 4.15 g (Yield from benzamide, 93%) of the title compound as a solid. were introduced into a 100 ml flask at normal temperature by means of a syringe, during which an exothermic reaction The resulting reaction mixture was refluxed for 5 hours cooled to normal temperature The reaction solvent and the excess oxalyl chloride were removed
来源 ID: ord-c94d970e9a6e47519ec71e9a98559b60反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: A mixture of 0.52 g of 2,6-difluorobenzamide and 0.33 ml of oxalyl chloride was stirred under reflux in 15 ml 1,2-dichloroethane overnight. Solvent was removed under vacuum and 10 ml 1,2-dichloroethane was added. Solvent was removed under vacuum to leave the title intermediate, which could be used directly or dissolved in 1,2-dichloroethane and stored for future use. Solvent was removed under vacuum and 10 ml 1,2-dichloroethane was added Solvent was removed under vacuum
来源 ID: ord-9ec64f802b00415fb4d96c17e72d0c18PubChem References
以下资料来自该化合物的公开数据库参考记录。