2-(4-氯苯基)乙胺盐酸盐

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A slurry of 15.9 g (0.08 mole) of p-chlorophenethylamine hydrochloride in 25 ml of O-methylcaprolactim is allowed to stand at room temperature 3 days with occasional stirring with a glass rod. The mixture is then cooled and the resulting solid is collected, washed with ether and recrystallized from methanol-acetone to give 2-(p-chlorophenylethylimino)hexahydroazapine hydrochloride. The mixture is then cooled the resulting solid is collected washed with ether recrystallized from methanol-acetone

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A slurry of 15.9 g (0.08 mole) of p-chlorophenethylamine hydrochloride in 25 ml of O-methylcaprolactim is allowed to stand at room temperature 3 days with occasional stirring with a glass rod. The mixture is then cooled and the resulting solid is collected, washed with ether and recrystallized from methanol-acetone to give 2-(p-chlorophenylethylimino)hexahydroazapine hydrochloride. The mixture is then cooled the resulting solid is collected washed with ether recrystallized from methanol-acetone

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A slurry of 15.9 g (0.08 mole) of p-chlorophenethylamine hydrochloride in 25 ml of O-methylcaprolactim is allowed to stand at room temperature 3 days with occasional stirring with a glass rod. The mixture is then cooled and the resulting solid is collected, washed with ether and recrystallized from methanol-acetone to give 2-(p-chlorophenylethylimino)hexahydroazapine hydrochloride. The mixture is then cooled the resulting solid is collected washed with ether recrystallized from methanol-acetone