反应 #3352271
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openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US05064945
反应条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: In 1.0 ml of water was dissolved 1.5 g of methylmalonic acid, after which 1.26 g of a 50% aqueous dimethylamine solution and 0.96 ml of a 37% aqueous formaldehyde solution were added with stirring at 0° C., and the resulting mixture was stirred at 0° to 5° C. for 3 hours and then at 80° C. for 30 minutes. the resulting mixture was stirred at 0° to 5° C. for 3 hours
来源 ID: ord-cc3d7a87fd854185b231c67ec2bf855a