1-octylsulfanyloctane

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Following the procedure and employing the reaction temperature and reactants of Example 7 with the exception that 53.5 grams (0.25 mole) of (C6H5CH2)2S were employed as a reactant instead of (n-C8H17)2S, 68 grams (53% yield)of C6H5CH2SP(S)Cl2 was obtained. The product had the following properties:

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Following the procedure of the preceding Examples, 64.5 grams (0.25 mole) of (n-C8H17)2S, 18.5 grams (0.0416 mole) of P4S10 and 90 grams (0.53 mole) of PSCl3 were reacted at 190° C for 10 hours. The crude reaction mixture was distilled twice to provide 68 grams (49% yield) of n-C8H17SP(S)Cl2 having the following properties: were reacted at 190° C for 10 hours The crude reaction mixture was distilled twice

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Following the procedure and employing the reaction temperature and reactants of Example 7 with the exception that 53.5 grams (0.25 mole) of (C6H5CH2)2S were employed as a reactant instead of (n-C8H17)2S, 68 grams (53% yield)of C6H5CH2SP(S)Cl2 was obtained. The product had the following properties:

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Following the procedure of the preceding Examples, 64.5 grams (0.25 mole) of (n-C8H17)2S, 18.5 grams (0.0416 mole) of P4S10 and 90 grams (0.53 mole) of PSCl3 were reacted at 190° C for 10 hours. The crude reaction mixture was distilled twice to provide 68 grams (49% yield) of n-C8H17SP(S)Cl2 having the following properties: were reacted at 190° C for 10 hours The crude reaction mixture was distilled twice