反应 #3382706
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openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US06054523
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: About 103 g of N-(2-aminoethyl)-3-aminopropylmethyldimethoxysilane (commercially available under the name "Silan GF 95" from Wacker-Chemie GmbH, Munich) are metered into a solution containing 63.7 g of potassium hydroxide (88% strength in water) in 200 g of water, while stirring vigorously. First methanol and then about 70 g of water are distilled off from the mixture by heating. The mixture is then made up to a total weight of 317 g by addition of water. A 40% potassium N-(2-aminoethyl)-3-aminopropylmethylsilanolate solution is obtained. First methanol and then about 70 g of water are distilled off from the mixture by heating The mixture is then made up to a total weight of 317 g by addition of water
来源 ID: ord-25a587ce62f94a16ae2f6b6abcbc7747