反应 #2849560
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openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US08497271B2
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: A solution of [(R)-1-(4-bromo-phenyl)-2-hydroxy-ethyl]-carbamic acid t-butyl ester (946 mg, 3 mmol) in MeOH (15 ml) was treated with HCl in dioxane (4 M, 15 ml) for 1.5 h. The mixture was concentrated to give the titled compound (755 mg, 100%) as a white solid. The mixture was concentrated
来源 ID: ord-a73a874f4f6e4c08883a880458021e51