反应 #1713127
相关文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US08389248B2
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: D-Fucose (6-deoxy D-galactose) was reduced [a composition in total of 500 ml containing D-fucose at 1% and 20 ml of the Raney-nickel catalyst] to produce D-fucitol (6-deoxy D-galactitol). FIG. 57(a) shows HPLC analysis results of D-fucose before reduction and FIG. 57(b) shows HPLC analysis results of 6-deoxy L-galactitol after the reduction. The optical rotation of 6-deoxy L-galactitol was +1.7, and FIG. 58 shows 13C NMR spectrum of 6-deoxy L-galactitol.
来源 ID: ord-5762e74bbce94cd5bdc2f97717ca399d