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9 条反应 · 9 篇文献
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 1-(4-Ethoxybutyl)-4-piperidone is prepared from 4-piperidone and 1-chloro-4-ethoxybutane essentially as described above in Example 38, Scheme C, step a.
来源 ID: ord-9bf12b78014b42fcb195931e3f0bff35反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 1-(4-Ethoxybutyl)-4-piperidone is prepared from 4-piperidone and 1-chloro-4-ethoxybutane essentially as described above in Example 38, Scheme C, step a.
来源 ID: ord-9bf12b78014b42fcb195931e3f0bff35反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: Norpethidine (15.63 g, 67 mmol), 4-ethoxybutylchloride (10.67 g, 70 mmol), Na2CO3 (7.77 g, 73 mmol), KI (0.6 g) and acetonitrile (150 ml) were heated under reflux and stirring for 72 h. The mixture was filtered and the solvent removed. The residue was dissolved in diethyl ether, and the solution washed with water and dried (MgSO4). Destillation yielded 17.9 g of base boiling at 160°-163° C./0.05 mm Hg. B.p. acc. to J. Chem. Soc. 3062 (1958) 180° C./1 mm Hg. Hydrochloride m.p. 143°-145° C. under reflux The mixture was filtered the solvent removed The residue was dissolved in diethyl ether the solution washed with water dried (MgSO4) Destillation yielded 17.9 g of base boiling at 160°-163° C./0.05 mm Hg 3062 (1958) 180° C./1 mm Hg
来源 ID: ord-f9d1676c42964943926696a83eab1022反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: Norpethidine (15.63 g, 67 mmol), 4-ethoxybutylchloride (10.67 g, 70 mmol), Na2CO3 (7.77 g, 73 mmol), KI (0.6 g) and acetonitrile (150 ml) were heated under reflux and stirring for 72 h. The mixture was filtered and the solvent removed. The residue was dissolved in diethyl ether, and the solution washed with water and dried (MgSO4). Destillation yielded 17.9 g of base boiling at 160°-163° C./0.05 mm Hg. B.p. acc. to J. Chem. Soc. 3062 (1958) 180° C./1 mm Hg. Hydrochloride m.p. 143°-145° C. under reflux The mixture was filtered the solvent removed The residue was dissolved in diethyl ether the solution washed with water dried (MgSO4) Destillation yielded 17.9 g of base boiling at 160°-163° C./0.05 mm Hg 3062 (1958) 180° C./1 mm Hg
来源 ID: ord-f9d1676c42964943926696a83eab1022反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: Norpethidine (15.63 g, 67 mmol), 4-ethoxybutylchloride (10.67 g, 70 mmol), Na2CO3 (7.77 g, 73 mmol), KI (0.6 g) and acetonitrile (150 ml) were heated under reflux and stirring for 72 h. The mixture was filtered and the solvent removed. The residue was dissolved in diethyl ether, and the solution washed with water and dried (MgSO4). Destillation yielded 17.9 g of base boiling at 160°-163° C./0.05 mm Hg. B.p. acc. to J. Chem. Soc. 3062 (1958) 180° C./1 mm Hg. Hydrochloride m.p. 143°-145° C. under reflux The mixture was filtered the solvent removed The residue was dissolved in diethyl ether the solution washed with water dried (MgSO4) Destillation yielded 17.9 g of base boiling at 160°-163° C./0.05 mm Hg 3062 (1958) 180° C./1 mm Hg
来源 ID: ord-352ed2c999c145d39e93b1de8b9e9709反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: Norpethidine (15.63 g, 67 mmol), 4-ethoxybutylchloride (10.67 g, 70 mmol), Na2CO3 (7.77 g, 73 mmol), KI (0.6 g) and acetonitrile (150 ml) were heated under reflux and stirring for 72 h. The mixture was filtered and the solvent removed. The residue was dissolved in diethyl ether, and the solution washed with water and dried (MgSO4). Destillation yielded 17.9 g of base boiling at 160°-163° C./0.05 mm Hg. B.p. acc. to J. Chem. Soc. 3062 (1958) 180° C./1 mm Hg. Hydrochloride m.p. 143°-145° C. under reflux The mixture was filtered the solvent removed The residue was dissolved in diethyl ether the solution washed with water dried (MgSO4) Destillation yielded 17.9 g of base boiling at 160°-163° C./0.05 mm Hg 3062 (1958) 180° C./1 mm Hg
来源 ID: ord-352ed2c999c145d39e93b1de8b9e9709反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: Norpethidine (15.63 g, 67 mmol), 4-ethoxybutylchloride (10.67 g, 70 mmol), Na2CO3 (7.77 g, 73 mmol), KI (0.6 g) and acetonitrile (150 ml) were heated under reflux and stirring for 72 h. The mixture was filtered and the solvent removed. The residue was dissolved in diethyl ether, and the solution washed with water and dried (MgSO4). Destillation yielded 17.9 g of base boiling at 160°-163° C./0.05 mm Hg. B.p. acc. to J. Chem. Soc. 3062 (1958) 180° C./1 mm Hg. Hydrochloride m.p. 143°-145° C. under reflux The mixture was filtered the solvent removed The residue was dissolved in diethyl ether the solution washed with water dried (MgSO4) Destillation yielded 17.9 g of base boiling at 160°-163° C./0.05 mm Hg 3062 (1958) 180° C./1 mm Hg
来源 ID: ord-352ed2c999c145d39e93b1de8b9e9709反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 1-(4-Ethoxybutyl)-4-piperidone is prepared from 4-piperidone and 1-chloro-4-ethoxybutane essentially as described above in Example 38, Scheme C, step a.
来源 ID: ord-9bf12b78014b42fcb195931e3f0bff35反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: Norpethidine (15.63 g, 67 mmol), 4-ethoxybutylchloride (10.67 g, 70 mmol), Na2CO3 (7.77 g, 73 mmol), KI (0.6 g) and acetonitrile (150 ml) were heated under reflux and stirring for 72 h. The mixture was filtered and the solvent removed. The residue was dissolved in diethyl ether, and the solution washed with water and dried (MgSO4). Destillation yielded 17.9 g of base boiling at 160°-163° C./0.05 mm Hg. B.p. acc. to J. Chem. Soc. 3062 (1958) 180° C./1 mm Hg. Hydrochloride m.p. 143°-145° C. under reflux The mixture was filtered the solvent removed The residue was dissolved in diethyl ether the solution washed with water dried (MgSO4) Destillation yielded 17.9 g of base boiling at 160°-163° C./0.05 mm Hg 3062 (1958) 180° C./1 mm Hg
来源 ID: ord-f9d1676c42964943926696a83eab1022PubChem References
以下资料来自该化合物的公开数据库参考记录。