3,3,4,4,4-PENTAFLUOROBUTENE-1

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Into a reaction vessel were put 200 g of methyldichlorosilane and the same amount of the same binary catalyst as in Example 1, followed by the addition of 242 g of 3,3,4,4,4-pentafluorobutene. After the completion of the reaction at 70° C under 6 atmospheres, the reaction product was subjected to distillation to produce 3,3,4,4,4-pentafluorobutylmethyldichlorosilane (Boiling point: 130° C) at the yield 91% of the theoretical. Into a reaction vessel were put After the completion of the reaction at 70° C under 6 atmospheres the reaction product was subjected to distillation

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Into a reaction vessel were put 200 g of methyldichlorosilane and the same amount of the same binary catalyst as in Example 1, followed by the addition of 242 g of 3,3,4,4,4-pentafluorobutene. After the completion of the reaction at 70° C under 6 atmospheres, the reaction product was subjected to distillation to produce 3,3,4,4,4-pentafluorobutylmethyldichlorosilane (Boiling point: 130° C) at the yield 91% of the theoretical. Into a reaction vessel were put After the completion of the reaction at 70° C under 6 atmospheres the reaction product was subjected to distillation

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Into a reaction vessel were put 200 g of methyldichlorosilane and the same amount of the same binary catalyst as in Example 1, followed by the addition of 242 g of 3,3,4,4,4-pentafluorobutene. After the completion of the reaction at 70° C under 6 atmospheres, the reaction product was subjected to distillation to produce 3,3,4,4,4-pentafluorobutylmethyldichlorosilane (Boiling point: 130° C) at the yield 91% of the theoretical. Into a reaction vessel were put After the completion of the reaction at 70° C under 6 atmospheres the reaction product was subjected to distillation

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Into a reaction vessel were put 200 g of methyldichlorosilane and the same amount of the same binary catalyst as in Example 1, followed by the addition of 242 g of 3,3,4,4,4-pentafluorobutene. After the completion of the reaction at 70° C under 6 atmospheres, the reaction product was subjected to distillation to produce 3,3,4,4,4-pentafluorobutylmethyldichlorosilane (Boiling point: 130° C) at the yield 91% of the theoretical. Into a reaction vessel were put After the completion of the reaction at 70° C under 6 atmospheres the reaction product was subjected to distillation