反应 #3279246
相关文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US07001967B2
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: In a one-liter autoclave were charged 400 ml of toluene as a polymerization solvent, 0.001 moles of perbutyl neodecanoate as a polymerization initiator, 0.42 moles of N-(2-methylphenyl)maleimide, and 4.05 moles of isobutene, and the mixture was subjected to polymerization reaction under a polymerization condition at a polymerization temperature of 60° C. for a polymerization time of 5 hours, to obtain N-(2-methylphenyl)maleimide-isobutene alternating copolymer. The thus obtained N-(2-methylphenyl)maleimide-isobutene alternating copolymer had a weight average molecular weight (Mw) (as reduced into standard polystyrene) of 160,000 and a molecular weight distribution (Mw/Mn), which is expressed by [(weight average molecular weight (Mw))/(number average molecular weight (Mn))], of 2.7. the mixture was subjected to polymerization reaction under a polymerization condition at a polymerization temperature of 60° C. for a polymerization time of 5 hours
来源 ID: ord-20cd0d7e689248e394b863043ba2525e