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CN(C)CCCC1=CC=C(C=C1)N产品信息
N-[3-(4-氨基苯基)丙基]-N,N-二甲基胺（CAS 42817-60-7）的产品身份、结构标识及相关反应资料，供化学中间体检索、研发和采购评估使用。
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8 条反应 · 8 篇文献
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: Prepared analogously to Example 89 by reacting 3-(1-ethoxy-1-phenyl-methylidene)-5-nitro-2-indolinone with 4-(3-dimethylaminopropyl)-aniline. Prepared analogously to Example 89
来源 ID: ord-7551716ec85944ea9e49bdd6cf410d41反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-57a850da78504f0187da5e69d0e82ba7反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-57a850da78504f0187da5e69d0e82ba7反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: A solution of 3-dimethylamino-1-(4-nitrophenyl)propan-1-one (hydrochloride, 0.25 g) in glacial acetic acid (10 ml) was adjusted to pH 1 with concentrated hydrochloric acid and, under nitrogen, palladium(II) hydroxide (20% on carbon, 0.1 g) was added. The nitrogen atmosphere was replaced by hydrogen, and the suspension was shaken for 6 hours. The catalyst was filtered off and the filtrate was concentrated. The residue was partitioned between saturated sodium bicarbonate solution and ethyl acetate. The aqueous phase was adjusted to pH>12 with sodium hydroxide solution and extracted with ethyl acetate. The combined organic phases were dried and concentrated. The product with the molecular weight of 178.28 (C11H18N2); MS (ESI): 179 ([M+H]+), was obtained in this way. The catalyst was filtered off the filtrate was concentrated The residue was partitioned between saturated sodium bicarbonate solution and ethyl acetate extracted with ethyl acetate The combined organic phases were dried concentrated MS (ESI): 179 ([M+H]+), was obtained in this way
来源 ID: ord-d1c893dcde0c458ba625815b6f249e74反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: A solution of 3-dimethylamino-1-(4-nitrophenyl)propan-1-one (hydrochloride, 0.25 g) in glacial acetic acid (10 ml) was adjusted to pH 1 with concentrated hydrochloric acid and, under nitrogen, palladium(II) hydroxide (20% on carbon, 0.1 g) was added. The nitrogen atmosphere was replaced by hydrogen, and the suspension was shaken for 6 hours. The catalyst was filtered off and the filtrate was concentrated. The residue was partitioned between saturated sodium bicarbonate solution and ethyl acetate. The aqueous phase was adjusted to pH>12 with sodium hydroxide solution and extracted with ethyl acetate. The combined organic phases were dried and concentrated. The product with the molecular weight of 178.28 (C11H18N2); MS (ESI): 179 ([M+H]+), was obtained in this way. The catalyst was filtered off the filtrate was concentrated The residue was partitioned between saturated sodium bicarbonate solution and ethyl acetate extracted with ethyl acetate The combined organic phases were dried concentrated MS (ESI): 179 ([M+H]+), was obtained in this way
来源 ID: ord-d1c893dcde0c458ba625815b6f249e74反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: Prepared analogously to Example 89 by reacting 3-(1-ethoxy-1-phenyl-methylidene)-5-nitro-2-indolinone with 4-(3-dimethylaminopropyl)-aniline. Prepared analogously to Example 89
来源 ID: ord-7551716ec85944ea9e49bdd6cf410d41反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: Prepared analogously to Example 89 by reacting 3-(1-ethoxy-1-phenyl-methylidene)-5-nitro-2-indolinone with 4-(3-dimethylaminopropyl)-aniline. Prepared analogously to Example 89
来源 ID: ord-7551716ec85944ea9e49bdd6cf410d41反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: A solution of 3-dimethylamino-1-(4-nitrophenyl)propan-1-one (hydrochloride, 0.25 g) in glacial acetic acid (10 ml) was adjusted to pH 1 with concentrated hydrochloric acid and, under nitrogen, palladium(II) hydroxide (20% on carbon, 0.1 g) was added. The nitrogen atmosphere was replaced by hydrogen, and the suspension was shaken for 6 hours. The catalyst was filtered off and the filtrate was concentrated. The residue was partitioned between saturated sodium bicarbonate solution and ethyl acetate. The aqueous phase was adjusted to pH>12 with sodium hydroxide solution and extracted with ethyl acetate. The combined organic phases were dried and concentrated. The product with the molecular weight of 178.28 (C11H18N2); MS (ESI): 179 ([M+H]+), was obtained in this way. The catalyst was filtered off the filtrate was concentrated The residue was partitioned between saturated sodium bicarbonate solution and ethyl acetate extracted with ethyl acetate The combined organic phases were dried concentrated MS (ESI): 179 ([M+H]+), was obtained in this way
来源 ID: ord-d1c893dcde0c458ba625815b6f249e74PubChem References
以下资料来自该化合物的公开数据库参考记录。