4-壬酮

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Hydroxylamine hydrochloride (2.1 g) was added to a solution of 1-azabicyclo[3.2.2.]nonan-4-one (2.77 g) in ethanol (30 ml) and the mixture was heated under reflux for 2 h. On cooling the reaction mixture to room temperature, the white solid was collected by filtration and dried in vacuo to give the title compound (2.84 g, 75%). under reflux for 2 h the white solid was collected by filtration dried in vacuo

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Hydroxylamine hydrochloride (2.1 g) was added to a solution of 1-azabicyclo[3.2.2.]nonan-4-one (2.77 g) in ethanol (30 ml) and the mixture was heated under reflux for 2 h. On cooling the reaction mixture to room temperature, the white solid was collected by filtration and dried in vacuo to give the title compound (2.84 g, 75%). under reflux for 2 h the white solid was collected by filtration dried in vacuo

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Hydroxylamine hydrochloride (2.1 g) was added to a solution of 1-azabicyclo[3.2.2.]nonan-4-one (2.77 g) in ethanol (30 ml) and the mixture was heated under reflux for 2 h. On cooling the reaction mixture to room temperature, the white solid was collected by filtration and dried in vacuo to give the title compound (2.84 g, 75%). under reflux for 2 h the white solid was collected by filtration dried in vacuo