2-(4-氯苯胺基)-1-苯基乙酮

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: After dissolving compound 12 (2.27 g, 14.7 mmol) in THF, compound 11 (1.5 g, 6.1 mmol) was added thereto. After the agitation for 2 hours at room temperature, three times extractions were carried out with EA and three times washings were carried out with brine. Water was removed by using Na2SO4 and distillation under the reduced pressure was carried out. After the removal of a junk by column chromatography (EA/HX= 1/9), the next reaction was followed as a crude condition. was added three times extractions Water was removed Na2SO4 and distillation under the reduced pressure After the removal of a junk by column chromatography (EA/HX= 1/9) the next reaction

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: After dissolving compound 12 (2.27 g, 14.7 mmol) in THF, compound 11 (1.5 g, 6.1 mmol) was added thereto. After the agitation for 2 hours at room temperature, three times extractions were carried out with EA and three times washings were carried out with brine. Water was removed by using Na2SO4 and distillation under the reduced pressure was carried out. After the removal of a junk by column chromatography (EA/HX= 1/9), the next reaction was followed as a crude condition. was added three times extractions Water was removed Na2SO4 and distillation under the reduced pressure After the removal of a junk by column chromatography (EA/HX= 1/9) the next reaction

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: After dissolving compound 12 (2.27 g, 14.7 mmol) in THF, compound 11 (1.5 g, 6.1 mmol) was added thereto. After the agitation for 2 hours at room temperature, three times extractions were carried out with EA and three times washings were carried out with brine. Water was removed by using Na2SO4 and distillation under the reduced pressure was carried out. After the removal of a junk by column chromatography (EA/HX= 1/9), the next reaction was followed as a crude condition. was added three times extractions Water was removed Na2SO4 and distillation under the reduced pressure After the removal of a junk by column chromatography (EA/HX= 1/9) the next reaction