1,3-DIPHENYL-1,3-PROPANEDIOL

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Synthetic procedure was identical with that described in synthetic example 42(3), except that benzoyl chloride was replaced by propionyl chloride, and 1,3-diphenyl-2-methyl-1,3-propandiol was replaced by 1,3-diphenyl-1,3-propandiol. 1HNMR: δ (ppm) 7.13-7.36(10H, ArH), 5.76(2H, CH), 2.5(4H, CH2), 2.11(2H, CH2), 1.1(6H, CH3)

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Synthetic procedure was identical with that described in synthetic example 42(3), except that benzoyl chloride was replaced by propionyl chloride, and 1,3-diphenyl-2-methyl-1,3-propandiol was replaced by 1,3-diphenyl-1,3-propandiol. 1HNMR: δ (ppm) 7.13-7.36(10H, ArH), 5.76(2H, CH), 2.5(4H, CH2), 2.11(2H, CH2), 1.1(6H, CH3)

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Synthetic procedure was identical with that described in synthetic example 42(3), except that benzoyl chloride was replaced by propionyl chloride, and 1,3-diphenyl-2-methyl-1,3-propandiol was replaced by 1,3-diphenyl-1,3-propandiol. 1HNMR: δ (ppm) 7.13-7.36(10H, ArH), 5.76(2H, CH), 2.5(4H, CH2), 2.11(2H, CH2), 1.1(6H, CH3)