反应 #3750399
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openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US06562827B1
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 3.0 g of intermediate compound 8a were reacted in 70 ml of DMF with 2.9 g of N-(2-methoxybenzyl)piperazine analogously to Example 8b in the presence of 5.7 g of potassium carbonate and a spatula tipful of 18-crown-6, 1.3 g (27%) of the product being obtained.
来源 ID: ord-df73b472d38549b88c863505e8777eea