反应 #1351373
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openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US08771660B2
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 16-Methyloctadecanoic acid was synthesized by the same operation, except that in the step (a) of the synthesis process for 14-methylhexadecanoic acid described above, 12-dodecanolide was changed to 15-pentadodecanolide, and in the step (b), 2-methylbutylmagnesium bromide was changed to sec-butylmagnesium bromide. Thus, 16-methyloctadecanoic add was obtained from 15-pentadodecanolide at a total yield of 84%. The purity was 95%. Thus, 16-methyloctadecanoic add
来源 ID: ord-dae4c3d7677b4b24b09047547b138a85