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CN(C)CCCOC1=CC=C(C=C1)N产品信息
4-(3-二甲基氨基丙氧基)苯胺（CAS 62424-88-8）的产品身份、结构标识及相关反应资料，供化学中间体检索、研发和采购评估使用。
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12 条反应 · 12 篇文献
反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-862625baa4894d0d994777a28d3819b0反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-d2067a658ea543228417a9877d1dd217反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-37c295f5e45746a1b59b7654a6b12903反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-ae3d6fbc53d842b18272e40690fd7679反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 4-(3-(dimethylamino)propoxy)nitrobenzene (4.4 g, 19.6 mmol) was hydrogenated over Pd (10% on C, 0.4 g) in ethanol (50 ml) for 16 h. The catalyst was filtered off and the solvent removed under reduced pressure to afford the title compound as a brown oil. MS (m/z)=195.3 (M+H+); Calc'd for C11H18N2O=194.28. The catalyst was filtered off the solvent removed under reduced pressure
来源 ID: ord-6c8632bc0a114664b7a78dd0642bbe76反应条件: temp:60.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: Palladium(II) hydroxide (20% on carbon; 0.4 g) was added to a solution of dimethyl-[3-(4-nitrophenoxy)propyl]amine (3.75 g) in ethanol (75 ml) under argon. Then formic acid (4 ml) was added dropwise, during which the reaction mixture heated to 60° C. while evolving much gas. After a reaction time of 90 minutes, the catalyst was filtered off and the filtrate was concentrated. The residue was partitioned between methyl tert-butyl ether and sodium hydroxide solution (2N). The organic phase was dried and concentrated. The product with the molecular weight of 194.28 (C11H18N2O); MS (ESI):195 ([M+H]+), was obtained in this way. After a reaction time of 90 minutes, the catalyst was filtered off the filtrate was concentrated The residue was partitioned between methyl tert-butyl ether and sodium hydroxide solution (2N) The organic phase was dried concentrated MS (ESI):195 ([M+H]+), was obtained in this way
来源 ID: ord-abea782cf2de4d93806b02fd7128ddc3反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 4-(3-(dimethylamino)propoxy)nitrobenzene (4.4 g, 19.6 mmol) was hydrogenated over Pd (10% on C, 0.4 g) in ethanol (50 ml) for 16 h. The catalyst was filtered off and the solvent removed under reduced pressure to afford the title compound as a brown oil. MS (m/z)=195.3 (M+H+); Calc'd for C11H18N2O=194.28. The catalyst was filtered off the solvent removed under reduced pressure
来源 ID: ord-18b5d0b13591476ebaa13d08e611dded反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 4-(3-(dimethylamino)propoxy)nitrobenzene (4.4 g, 19.6 mmol) was hydrogenated over Pd (10% on C, 0.4 g) in ethanol (50 ml) for 16 h. The catalyst was filtered off and the solvent removed under reduced pressure to afford the title compound as a brown oil. MS (m/z)=195.3 (M+H+); Calc'd for C11H18N2O=194.28. The catalyst was filtered off the solvent removed under reduced pressure
来源 ID: ord-18b5d0b13591476ebaa13d08e611dded反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-862625baa4894d0d994777a28d3819b0反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-d2067a658ea543228417a9877d1dd217反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-37c295f5e45746a1b59b7654a6b12903反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-ae3d6fbc53d842b18272e40690fd7679PubChem References
以下资料来自该化合物的公开数据库参考记录。