反应 #2525088
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openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US07091230B2
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: Sodium propanoate (0.88 g, 1.5 eq) and 2,6-dipropylphenol (1.09 g, 1.0 eq) were combined in Triflic Acid (5.0 g) as in Example 13, step 1. The resulting waxy solid was purified by chromatography on silica gel using ethyl acetate:hexanes:acetic acid (10:90:1) to give the titled phenol. The resulting waxy solid was purified by chromatography on silica gel
来源 ID: ord-ec11d9e4f3f449f6a915145c8ea66bec