反应 #1244659
相关文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US09018175B2
反应条件: temp:100.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: A mixture of propoxyacetonitrile (3.03 g) and hydroxylamine (2.01 g, 50 wt % in water) is stirred for 2 h at 100° C. At RT DCM is added, the organic phase is separated, dried over sodium sulfate and concentrated under reduced pressure to give the title compound as an oil. the organic phase is separated dried over sodium sulfate concentrated under reduced pressure
来源 ID: ord-1489afd5ce5c4c1e95fdd821af9fbff7