反应 #99941
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openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US08524702B2
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: A solution of tert-butyl 2-hydroxybenzyl(propyl)carbamate (89 g, 0.34 mol) in MeOH (400 mL) was bubbled with HCl gas. After stirring for 5 h at room temperature, the reaction mixture was concentrated under reduced pressure to afford 61 g (90%) of 2-((propylamino)methyl)phenol as HCl salt. the reaction mixture was concentrated under reduced pressure
来源 ID: ord-1773d168b0c04d3cb8c937689a385a1d