反应 #1005057
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openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US04906402
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: This was prepared by the methods of Examples 2(b) and 2(c) using butanol instead of propanol and using 4-(3-chloro-4-octoxyphenyl)benzoyl chloride and Butyl (R)-2-(4-hydroxyphenoxy)propanoate (BHPP) in place of the OPBC and PHPTB used in Example 2(c), (yield 15%, SOR: +16°). The results of IR, 1H-NMR and mass spectroscopy and elemental analysis were consistent with the assigned structure. used in Example 2(c), (yield 15%, SOR: +16°) The results of IR, 1H-NMR and mass spectroscopy and elemental analysis
来源 ID: ord-1c4cc12767284f63b88dbba1b5afa74c