反应 #3478381
相关文献 (1)
openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US04393217
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: As for Example 1, 2-cyano-2',5'-difluoroacetanilide, colorless crystals, m.p. 165°-167° C. (prepared by the procedure described in U.S. Pat. No. 3,116,312), is heated with N,N-dimethylformamide dimethylacetal to give 2-cyano-3-dimethylamino-2',5'-difluoroacrylanilide as colorless needles, m.p. 175°-176° C.
来源 ID: ord-8a485297efbb4438a1749904943f922f