反应 #1245916
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openreactiondata ↗doi:10.6084/m9.figshare.5104873.v1; patent:US09403808B2
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: The title compound was synthesized in analogy to Example 69 using 5-cyclopropyl-6-cyclopropylmethoxy-pyrazine-2-carboxylic acid (Example 10 g, 50 mg, 0.214 mmol) and 3-methoxy-1,1-dimethyl-propylamine (CAN 889765-21-3, 50 mg, 0.32 mmol) as starting materials and isolated (40 mg, 56.14%) as white solid; LC-MS (UV peak area, ESI) 99.87%, 333.8 (M+H)+. isolated (40 mg, 56.14%) as white solid
来源 ID: ord-627167c854cd4822bfbb0b656338fd9c