1-吡咯烷-1-基丁-2-烯-1-one

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Following the procedure of Example 4, 2,6-bis(1,1-dimethylethyl)-4-mercaptophenol (2.Og, 0.008 mole) and 1-(1-oxo-2-butenyl)pyrrolidine (1.llg, 0.008 mole) were dissolved in methanol (20ml) under an argon atmosphere and refluxed for 24 hours. The solvent was removed and the product isolated by chromatography on silica, and recrystallized from hexane to yield the product as a white solid, m.p. about 95°-99° C. refluxed for 24 hours The solvent was removed the product isolated by chromatography on silica recrystallized from hexane

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: 3-Methylacryloyl chloride was reacted with pyrrolidine by the method of Example 14 to give the title amide.

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Following the procedure of Example 4, 2,6-bis(1,1-dimethylethyl)4-mercaptophenol (2.0 g. 0.008 mole) and 1(1-oxo-2-butenyl)pyrrolidine (1.11 g, 0.008 mole) were dissolved in methanol (20 ml) under an argon atmosphere and refluxed for 24 hours. The solvent was removed and the product isolated by chromatography on silica, and recrystallized from hexane to yield the product as a white solid, m.p. about 95°-99° C. refluxed for 24 hours The solvent was removed the product isolated by chromatography on silica recrystallized from hexane

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: 3-Methylacryloyl chloride was reacted with pyrrolidine by the method of Example 14 to give the title amide.

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: 3-Methylacryloyl chloride was reacted with pyrrolidine by the method of Example 14 to give the title amide.

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Following the procedure of Example 4, 2,6-bis(1,1-dimethylethyl)-4-mercaptophenol (2.Og, 0.008 mole) and 1-(1-oxo-2-butenyl)pyrrolidine (1.llg, 0.008 mole) were dissolved in methanol (20ml) under an argon atmosphere and refluxed for 24 hours. The solvent was removed and the product isolated by chromatography on silica, and recrystallized from hexane to yield the product as a white solid, m.p. about 95°-99° C. refluxed for 24 hours The solvent was removed the product isolated by chromatography on silica recrystallized from hexane

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: 3-Methylacryloyl chloride was reacted with pyrrolidine by the method of Example 14 to give the title amide.

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Following the procedure of Example 4, 2,6-bis(1,1-dimethylethyl)4-mercaptophenol (2.0 g. 0.008 mole) and 1(1-oxo-2-butenyl)pyrrolidine (1.11 g, 0.008 mole) were dissolved in methanol (20 ml) under an argon atmosphere and refluxed for 24 hours. The solvent was removed and the product isolated by chromatography on silica, and recrystallized from hexane to yield the product as a white solid, m.p. about 95°-99° C. refluxed for 24 hours The solvent was removed the product isolated by chromatography on silica recrystallized from hexane

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: 3-Methylacryloyl chloride was reacted with pyrrolidine by the method of Example 14 to give the title amide.