N-(4-氨基-2-甲基苯基)-2-氟苯甲酰胺

反应条件: temp:0.00; pressure:0.00; stir:

反应条件: temp:4.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A mixture of 2-fluoro-N-(2-methyl-4-nitrophenyl)benzamide (4.55 g), cyclohexene (30 mL), ethanol (70 mL), water (30 mL) and 10% palladium on charcoal (3 g) is heated at reflux for 30 minutes. The mixture is filtered through diatomaceous earth and concentrated under reduced pressure. The resulting oil is dissolved in 50 mL of ethyl acetate and cooled at 4° C. for 12 hours. Filtration provides the product as a tan solid. is heated at reflux for 30 minutes The mixture is filtered through diatomaceous earth concentrated under reduced pressure The resulting oil is dissolved in 50 mL of ethyl acetate Filtration

反应条件: temp:0.00; pressure:0.00; stir:

反应条件: temp:4.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A mixture of 2-fluoro-N-(2-methyl-4-nitrophenyl)benzamide (4.55 g), cyclohexene (30 mL), ethanol (70 mL), water (30 mL) and 10% palladium on charcoal (3 g) is heated at reflux for 30 minutes. The mixture is filtered through diatomaceous earth and concentrated under reduced pressure. The resulting oil is dissolved in 50 mL of ethyl acetate and cooled at 4° C. for 12 hours. Filtration provides the product as a tan solid. is heated at reflux for 30 minutes The mixture is filtered through diatomaceous earth concentrated under reduced pressure The resulting oil is dissolved in 50 mL of ethyl acetate Filtration

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A mixture of 2-fluoro-N-(2-methyl-4-nitrophenyl)benzamide (4.55 g), cyclohexene (30 mL), ethanol (70 mL), water (30 mL) and 10% palladium on charcoal (3 g) is heated at reflux for 30 minutes. The mixture is filtered through diatomaceous earth and concentrated under reduced pressure. The resulting oil is dissolved in 50 mL of ethyl acetate and cooled at 40 C for 12 hours. Filtration provides the product as a tan solid. is heated at reflux for 30 minutes The mixture is filtered through diatomaceous earth concentrated under reduced pressure The resulting oil is dissolved in 50 mL of ethyl acetate cooled at 40 C for 12 hours Filtration

反应条件: temp:4.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A mixture of 2-fluoro-N-(2-methyl-4-nitrophenyl)benzamide (4.55 g), cyclohexene (30 mL), ethanol (70 mL), water (30 mL) and 10% palladium on charcoal (3 g) is heated at reflux for 30 minutes. The mixture is filtered through diatomaceous earth and concentrated under reduced pressure. The resulting oil is dissolved in 50 niL of ethyl acetate and cooled at 4° C. for 12 hours. Filtration provides the product as a tan solid. is heated at reflux for 30 minutes The mixture is filtered through diatomaceous earth concentrated under reduced pressure The resulting oil is dissolved in 50 niL of ethyl acetate Filtration

反应条件: temp:4.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A mixture of 2-fluoro-N-(2-methyl-4-nitrophenyl)benzamide (4.55 g), cyclohexene (30 mL), ethanol (70 mL), water (30 mL) and 10% palladium on charcoal (3 g) is heated at reflux for 30 minutes. The mixture is filtered through diatomaceous earth and concentrated under reduced pressure. The resulting oil is dissolved in 50 mL of ethyl acetate and cooled at 4° C. for 12 hours. Filtration provides the product as a tan solid. is heated at reflux for 30 minutes The mixture is filtered through diatomaceous earth concentrated under reduced pressure The resulting oil is dissolved in 50 mL of ethyl acetate Filtration

反应条件: temp:4.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A mixture of 2-fluoro-N-(2-methyl-4-nitrophenyl)benzamide (4.55 g), cyclohexene (30 mL), ethanol (70 mL), water (30 mL) and 10% palladium on charcoal (3 g) is heated at reflux for 30 minutes. The mixture is filtered through diatomaceous earth and concentrated under reduced pressure. The resulting oil is dissolved in 50 mL of ethyl acetate and cooled at 4° C. for 12 hours. Filtration provides the product as a tan solid. is heated at reflux for 30 minutes The mixture is filtered through diatomaceous earth concentrated under reduced pressure The resulting oil is dissolved in 50 mL of ethyl acetate Filtration

反应条件: temp:4.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A mixture of 2-fluoro-N-(2-methyl-4-nitrophenyl)benzamide (4.55 g), cyclohexene (30 mL), ethanol (70 mL), water (30 mL) and 10% palladium on charcoal (3 g) is heated at reflux for 30 minutes. The mixture is filtered through diatomaceous earth and concentrated under reduced pressure. The resulting oil is dissolved in 50 mL of ethyl acetate and cooled at 4° C. for 12 hours. Filtration provides the product as a tan solid. is heated at reflux for 30 minutes The mixture is filtered through diatomaceous earth concentrated under reduced pressure The resulting oil is dissolved in 50 mL of ethyl acetate Filtration

反应条件: temp:4.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A mixture of 2-fluoro-N-(2-methyl-4-nitrophenyl)benzamide (4.55 g), cyclohexene (30 mL), ethanol (70 mL), water (30 mL) and 10% palladium on charcoal (3 g) is heated at reflux for 30 minutes. The mixture is filtered through diatomaceous earth and concentrated under reduced pressure. The resulting oil is dissolved in 50 mL of ethyl acetate and cooled at 4° C. for 12 hours. Filtration provides the product as a tan solid. is heated at reflux for 30 minutes The mixture is filtered through diatomaceous earth concentrated under reduced pressure The resulting oil is dissolved in 50 mL of ethyl acetate Filtration

反应条件: temp:4.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A mixture of 2-fluoro-N-(2-methyl-4-nitrophenyl)benzamide (4.55 g), cyclohexene (30 mL), ethanol (70 mL), water (30 mL) and 10% palladium on charcoal (3 g) is heated at reflux for 30 minutes. The mixture is filtered through diatomaceous earth and concentrated under reduced pressure. The resulting oil is dissolved in 50 mL of ethyl acetate and cooled at 4° C. for 12 hours. Filtration provides the product as a tan solid. is heated at reflux for 30 minutes The mixture is filtered through diatomaceous earth concentrated under reduced pressure The resulting oil is dissolved in 50 mL of ethyl acetate Filtration

反应条件: temp:4.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A mixture of 2-fluoro-N-(2-methyl-4-nitrophenyl)benzamide (4.55 g), cyclohexene (30 mL), ethanol (70 mL), water (30 mL) and 10% palladium on charcoal (3 g) is heated at reflux for 30 minutes. The mixture is filtered through diatomaceous earth and concentrated under reduced pressure. The resulting oil is dissolved in 50 mL of ethyl acetate and cooled at 4° C. for 12 hours. Filtration provides the product as a tan solid. is heated at reflux for 30 minutes The mixture is filtered through diatomaceous earth concentrated under reduced pressure The resulting oil is dissolved in 50 mL of ethyl acetate Filtration