四氟硼酸甲基联苯硫酯

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A solution of methyldiphenylsulfonium tetrafluoroborate, [(CH3)(C6H5)2S][BF4], (4.50 g, 30.69 mmol), 100 mg, 0.347 mmol in acetonitrile (2 ml) and a solution of potassium methyltricyanoborate (50 mg, 0.347 mmol in acetonitril (2 ml) are combined and mixed. The salt potassium tetrafluoroborate is filtered at 0° C. and all volatile components are removed under reduced pressure resulting in the compound methyldiphenylsulfonium methyltricyanoborate. mixed The salt potassium tetrafluoroborate is filtered at 0° C. all volatile components are removed under reduced pressure