[(1S,3S,4S)-4-氨基-3-羟基-5-苯基-1-(苯甲基)戊基]-氨基甲酸叔丁酯

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A slurry obtained by mixing 6.2 g of a borosilicate glass powder, 56.0 g of nickel-zinc ferrite, 6.2 g of an acrylic organic binder containing hydroxyl groups, 3.1 g of ethanol, 3.0 g of trimethylolpropane triacrylate, 1.2 g of 2-methyl-1-[4-(methylthio)phenyl]-2-morphorinopropane-1-on, 0.3 g of 2,4-diethylthioxanthone and 0.5 g of dipropyleneglycol monomethyl ether was formed into a sheet by the doctor blade method. The sheet was dried at 100° C. to obtain a photosensitive magnetic ceramic green sheet with a thickness of 30 μm. A slurry obtained

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A slurry obtained by mixing 6.2 g of a borosilicate glass powder, 56.0 g of barium titanate, 6.2 g of an acrylic organic binder containing hydroxyl groups, 3.1 g of ethanol, 3.0 g of trimethylolpropane triacrylate, 1.2 g of 2-methyl-1-[4-(methylthio)phenyl]-2-morphorinopropane-1-on, 0.3 g of 2,4-diethylthioxanthone and 0.5 g of dipropyleneglycol monomethyl ether was formed into a sheet by the doctor blade method. The sheet was dried at 100° C. to obtain a photosensitive dielectric ceramic green sheet with a thickness of 30 μm. A slurry obtained

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A slurry obtained by mixing 37.7 g of a borosilicate glass powder, 24.9 g of alumina powder, 6.2 g of an acrylic organic binder containing hydroxyl groups, 3.1 g of ethanol, 3.0 g of trimethylolpropane triacrylate, 1.2 g of 2-methyl-1-[4-(methylthio)phenyl]2-morphorinopropane-1-on, 0.3 g of 2,4-diethylthioxanthone and 0.5 g of dipropyleneglycol monomethyl ether was formed into a sheet by the doctor blade method. The sheet was dried at 100° C. to obtain a photosensitive insulating ceramic green sheet with a thickness of 30 μm. A slurry obtained by mixing 37.7 g of a borosilicate glass powder, 24.9 g of alumina powder, 6.2 g of an acrylic organic binder

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A slurry obtained by mixing 37.7 g of a borosilicate glass powder, 24.9 g of alumina powder, 6.2 g of an acrylic organic binder containing hydroxyl groups, 3.1 g of ethanol, 3.0 g of trimethylolpropane triacrylate, 1.2 g of 2-methyl-1-[4-(methylthio)phenyl]2-morphorinopropane-1-on, 0.3 g of 2,4-diethylthioxanthone and 0.5 g of dipropyleneglycol monomethyl ether was formed into a sheet by the doctor blade method. The sheet was dried at 100° C. to obtain a photosensitive insulating ceramic green sheet with a thickness of 30 μm. A slurry obtained by mixing 37.7 g of a borosilicate glass powder, 24.9 g of alumina powder, 6.2 g of an acrylic organic binder

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: In the DOWANOL PPH preparation above, substitute 18 g of 25% DCOIT in DOWANOL DPM (final concentration of 1500 ppm DCOIT) stirring as directed.

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: In the DOWANOL PPH preparation above, substitute 18 g of 25% DCOIT in DOWANOL DPM (final concentration of 1500 ppm DCOIT) stirring as directed.

反应条件: temp:130.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: An autoclave, as equipped with a thermometer, a stirrer, and a nitrogen-introducing tube, was charged with 74 parts by weight of dipropylene glycol monomethyl ether and 1 part by weight of sodium hydroxide powder, and the internal air of the autoclave was displaced with nitrogen, and then the charged materials were heated to 130° C. Next, 426 parts by weight of ethylene oxide was introduced into the autoclave over a period of 3 hours, and then the resultant reaction mixture was aged at 130° C. for 2 hours and then cooled, thus obtaining a dipropylene glycol monomethyl ether-ethylene oxide adduct (number-average molecular weight=1,000, average molar number of addition=1.94). An autoclave, as equipped with a thermometer, a stirrer a nitrogen-introducing tube the resultant reaction mixture cooled

反应条件: temp:130.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: An autoclave, as equipped with a thermometer, a stirrer, and a nitrogen-introducing tube, was charged with 74 parts by weight of dipropylene glycol monomethyl ether and 1 part by weight of sodium hydroxide powder, and the internal air of the autoclave was displaced with nitrogen, and then the charged materials were heated to 130° C. Next, 426 parts by weight of ethylene oxide was introduced into the autoclave over a period of 3 hours, and then the resultant reaction mixture was aged at 130° C. for 2 hours and then cooled, thus obtaining a dipropylene glycol monomethyl ether-ethylene oxide adduct (number-average molecular weight=1,000, average molar number of addition=1.94). An autoclave, as equipped with a thermometer, a stirrer a nitrogen-introducing tube the resultant reaction mixture cooled

反应条件: temp:130.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: An autoclave, as equipped with a thermometer, a stirrer, and a nitrogen-introducing tube, was charged with 74 parts by weight of dipropylene glycol monomethyl ether and 1 part by weight of sodium hydroxide powder, and the internal air of the autoclave was displaced with nitrogen, and then the charged materials were heated to 130° C. Next, 426 parts by weight of ethylene oxide was introduced into the autoclave over a period of 3 hours, and then the resultant reaction mixture was aged at 130° C. for 2 hours and then cooled, thus obtaining a dipropylene glycol monomethyl ether-ethylene oxide adduct (number-average molecular weight=1,000, average molar number of addition=1.94). An autoclave, as equipped with a thermometer, a stirrer a nitrogen-introducing tube the resultant reaction mixture cooled

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A slurry obtained by mixing 37.3 g of borosilicate glass powder, 24.9 g of alumina powder, 6.2 g of copolymer (weight average molecular weight=50,000) having a methacrylic acid/methyl methacrylate copolymerization ratio of 25/75 by weight, 3.1 g of ethanol and 0.5 g of dipropylene glycol monomethyl ether was formed in a sheet by the doctor blade method, and then dried at 100° C. for 1 hour to obtain a ceramic green sheet having a thickness of 30 μm. A slurry obtained

反应条件: temp:100.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Dipropylene glycol monomethyl ether (444.6 grams; 3.0 mol), benzoic acid (373.7 grams; 3.06 mol), toluene (50 ml) and zirconium carbonate (2.0 grams) were placed into a 200 ml, 3-necked round bottom flask equipped with stirrer, thermometer, heating mantle, Dean Stark water trap, condenser and 10" Vigneux column. The reaction temperature was 180° C. at the beginning of the reaction and 217° C. after 6.5 hours with stirring. During that time, water (44 mls) was removed. The reaction was continued the next day for 2.5 hours at 224°-226° C. with the removal of water (56 mls.). The reaction mixture was washed at 95°-100° C. three times with sodium carbonate (15%) and then washed with water (400 ml). Then additional water (200 ml) was added and the product separated and dried at 125°, cooled to 100° C. and filtered. The desired product (694.6 grams) was obtained representing a yield of 91.8%. It assayed 99.5% with the following properties: equipped with stirrer The reaction temperature was 180° C. at the beginning of the reaction and 217° C. after 6.5 hours During that time, water (44 mls) was removed for 2.5 hours at 224°-226° C. with the removal of water (56 mls.) The reaction mixture was washed at 95°-100° C. three times with sodium carbonate (15%) washed with water (400 ml) Then additional water (200 ml) was added the product separated dried at 125° filtered

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: A slurry obtained by mixing 6.2 g of a borosilicate glass powder, 56.0 g of nickel-zinc ferrite, 6.2 g of an acrylic organic binder containing hydroxyl groups, 3.1 g of ethanol, 3.0 g of trimethylolpropane triacrylate, 1.2 g of 2-methyl-1-[4-(methylthio)phenyl]-2-morphorinopropane-1-on, 0.3 g of 2,4-diethylthioxanthone and 0.5 g of dipropyleneglycol monomethyl ether was formed into a sheet by the doctor blade method. The sheet was dried at 100° C. to obtain a photosensitive magnetic ceramic green sheet with a thickness of 30 μm. A slurry obtained