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2-(环戊氧基)苯甲醛（CAS 145742-38-7）的产品身份、结构标识及相关反应资料，供化学中间体检索、研发和采购评估使用。
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10 条反应 · 10 篇文献
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: The title compound was prepared from 2-cyclopentyloxybenzaldehyde, 3-aminopyrazole and ethyl 3-ketohexanoate in the same manner as in Example 25.
来源 ID: ord-39a0d3a811d04de49dc9804f76e2a630反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: The title compound was prepared from 2-cyclopentyloxybenzaldehyde, 3-aminopyrazole and ethyl 3-ketohexanoate in the same manner as in Example 25.
来源 ID: ord-39a0d3a811d04de49dc9804f76e2a630反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 77.70 g (500 mmoles) of isovanilin and 69.40 g (600 mmoles) of 97% potassium t-butoxide (t-BuOK) dissolved in 800 ml of 1-propanol, 69.0 ml 630 mmoles), and the solution refluxed. After 3 hours another 9.25 g (80 mmoles) of t-BuOK were added at 80° C. and the suspension refluxed for another 3 hours. The solid was filtered off and the filtrate evaporated in vacuo to dryness. The residue was dissolved in ether and extracted with 1N NaOH. The ether phase was evaporated to dryness: 85.40 g (77.5%) of cyclopentyloxybenzaldehyde was isolated. 69.0 ml 630 mmoles), and the solution refluxed the suspension refluxed for another 3 hours The solid was filtered off the filtrate evaporated in vacuo to dryness The residue was dissolved in ether extracted with 1N NaOH The ether phase was evaporated to dryness
来源 ID: ord-2a86e40e6eb44b2c97dac082f4591e3a反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 77.70 g (500 mmoles) of isovanilin and 69.40 g (600 mmoles) of 97% potassium t-butoxide (t-BuOK) dissolved in 800 ml of 1-propanol, 69.0 ml 630 mmoles), and the solution refluxed. After 3 hours another 9.25 g (80 mmoles) of t-BuOK were added at 80° C. and the suspension refluxed for another 3 hours. The solid was filtered off and the filtrate evaporated in vacuo to dryness. The residue was dissolved in ether and extracted with 1N NaOH. The ether phase was evaporated to dryness: 85.40 g (77.5%) of cyclopentyloxybenzaldehyde was isolated. 69.0 ml 630 mmoles), and the solution refluxed the suspension refluxed for another 3 hours The solid was filtered off the filtrate evaporated in vacuo to dryness The residue was dissolved in ether extracted with 1N NaOH The ether phase was evaporated to dryness
来源 ID: ord-2a86e40e6eb44b2c97dac082f4591e3a反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 77.70 g (500 mmoles) of isovanillin and 69.40 g (600 mmoles) of 97% potassium t-butoxide (t-BuOK) dissolved in 800 ml of 1-propanol, 69.0 ml 630 mmoles), and the solution refluxed. After 3 hours another 9.25 g (80 mmoles) of t-BuOK were added at 80° C. and the suspension refluxed for another 3 hours. The solid was filtered off and the filtrate evaporated in vacuo to dryness. The residue was dissolved in ether and extracted with 1N NaOH. The ether phase was evaporated to dryness: 85.40 g (77.5%) of cyclopentyloxybenzaldehyde was isolated. 69.0 ml 630 mmoles), and the solution refluxed the suspension refluxed for another 3 hours The solid was filtered off the filtrate evaporated in vacuo to dryness The residue was dissolved in ether extracted with 1N NaOH The ether phase was evaporated to dryness
来源 ID: ord-4e3f3970edc94e6e9c8dc563cecca0a1反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 77.70 g (500 mmoles) of isovanillin and 69.40 g (600 mmoles) of 97% potassium t-butoxide (t-BuOK) dissolved in 800 ml of 1-propanol, 69.0 ml 630 mmoles), and the solution refluxed. After 3 hours another 9.25 g (80 mmoles) of t-BuOK were added at 80° C. and the suspension refluxed for another 3 hours. The solid was filtered off and the filtrate evaporated in vacuo to dryness. The residue was dissolved in ether and extracted with 1N NaOH. The ether phase was evaporated to dryness: 85.40 g (77.5%) of cyclopentyloxybenzaldehyde was isolated. 69.0 ml 630 mmoles), and the solution refluxed the suspension refluxed for another 3 hours The solid was filtered off the filtrate evaporated in vacuo to dryness The residue was dissolved in ether extracted with 1N NaOH The ether phase was evaporated to dryness
来源 ID: ord-4e3f3970edc94e6e9c8dc563cecca0a1反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 77.70 g (500 mmoles) of isovanillin and 69.40 g (600 mmoles) of 97% potassium t-butoxide (t-BuOK) dissolved in 800 ml of 1-propanol, 69.0 ml 630 mmoles), and the solution refluxed. After 3 hours another 9.25 g (80 mmoles) of t-BuOK were added at 80° C. and the suspension refined for another 3 hours. The solid was filtered off and the filtrate evaporated in vacuo to dryness. The residue was dissolved in ether and extracted with 1N NaOH. The ether phase was evaporated to dryness: 85.40 g (77.5%) of cyclopentyloxybenzaldehyde was isolated. 69.0 ml 630 mmoles), and the solution refluxed The solid was filtered off the filtrate evaporated in vacuo to dryness The residue was dissolved in ether extracted with 1N NaOH The ether phase was evaporated to dryness
来源 ID: ord-bec6ffbb5c1c4e3d9cd950fda28d4013反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 77.70 g (500 mmoles) of isovanillin and 69.40 g (600 mmoles) of 97% potassium t-butoxide (t-BuOK) dissolved in 800 ml of 1-propanol, 69.0 ml 630 mmoles), and the solution refluxed. After 3 hours another 9.25 g (80 mmoles) of t-BuOK were added at 80° C. and the suspension refluxed for another 3 hours. The solid was filtered off and the filtrate evaporated in vacuo to dryness. The residue was dissolved in ether and extracted with IN NaOH. The ether phase was evaporated to dryness: 85.40 g (77.5%) of cyclopentyloxybenzaldehyde was isolated. 69.0 ml 630 mmoles), and the solution refluxed the suspension refluxed for another 3 hours The solid was filtered off the filtrate evaporated in vacuo to dryness The residue was dissolved in ether extracted with IN NaOH The ether phase was evaporated to dryness
来源 ID: ord-3ed661963d4d4676aa5d421bfc66bcea反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: The title compound was prepared from 2-cyclopentyloxybenzaldehyde, 3-aminopyrazole and ethyl 3-ketohexanoate in the same manner as in Example 25.
来源 ID: ord-39a0d3a811d04de49dc9804f76e2a630反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 77.70 g (500 mmoles) of isovanilin and 69.40 g (600 mmoles) of 97% potassium t-butoxide (t-BuOK) dissolved in 800 ml of 1-propanol, 69.0 ml 630 mmoles), and the solution refluxed. After 3 hours another 9.25 g (80 mmoles) of t-BuOK were added at 80° C. and the suspension refluxed for another 3 hours. The solid was filtered off and the filtrate evaporated in vacuo to dryness. The residue was dissolved in ether and extracted with 1N NaOH. The ether phase was evaporated to dryness: 85.40 g (77.5%) of cyclopentyloxybenzaldehyde was isolated. 69.0 ml 630 mmoles), and the solution refluxed the suspension refluxed for another 3 hours The solid was filtered off the filtrate evaporated in vacuo to dryness The residue was dissolved in ether extracted with 1N NaOH The ether phase was evaporated to dryness
来源 ID: ord-2a86e40e6eb44b2c97dac082f4591e3aPubChem References
以下资料来自该化合物的公开数据库参考记录。