2-(5-氯-2-(甲硫基)苯基)-4,4,5,5-四甲基-1,3,2-二恶硼烷

反应条件: temp:55.01; pressure:0.00; stir:

实验步骤: dtbpy: A mixture of ortho- and meta-borylated products (102 mg, 71% yield, ortho/meta + para = 2.0); white solid;

反应条件: temp:55.01; pressure:0.00; stir:

实验步骤: Ligand 3f: A mixture of ortho- and meta-borylated products (114 mg, 80% yield, ortho/meta + para = 12); ortho-borylated product 4e was obtained by further purification by GPC (70 mg, 49% yield), white solid (mp. 80-82 oC);