1,2-二氯四氟环丁-1-烯

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: 200 g (5 mol) of powdered sodium hydroxide are metered into a solution of 786 g (3.94 mol) of 1,2-dichloro-3,3,4,4-tetrafluorocyclobutene and 328 g (5.47 mol) of technical grade isopropanol at -10° C. The mixture is stirred for a further 2 hours, the solid is filtered off with suction and the filtrate is distilled. the solid is filtered off with suction the filtrate is distilled