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(3-氯-2-氟苯基)肼（CAS 396075-11-9）的产品身份、结构标识及相关反应资料，供化学中间体检索、研发和采购评估使用。
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10 条反应 · 10 篇文献
反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: The title compound, EI-MS: m/e=258.1 (M+), was prepared in accordance with the general method of example 25b) from (3-Chloro-2-fluoro-phenyl)-hydrazine and ethyl pyruvate.
来源 ID: ord-0a6950f5e4564622885e8b8ed23d9643反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: The title compound, EI-MS: m/e=258.1 (M+), was prepared in accordance with the general method of example 25b) from (3-Chloro-2-fluoro-phenyl)-hydrazine and ethyl pyruvate.
来源 ID: ord-0a6950f5e4564622885e8b8ed23d9643反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: The title compound, EI-MS: m/e=258.1 (M+), was prepared in accordance with the general method of example 25b) from (3-Chloro-2-fluoro-phenyl)-hydrazine and ethyl pyruvate.
来源 ID: ord-fcdfbf94bd5a467d81576a3da1a93570反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: The title compound, EI-MS: m/e=258.1 (M+), was prepared in accordance with the general method of example 25b) from (3-Chloro-2-fluoro-phenyl)-hydrazine and ethyl pyruvate.
来源 ID: ord-fcdfbf94bd5a467d81576a3da1a93570反应条件: temp:120.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: A mixture of 4-butyryl-2-hydroxy-benzoic acid methyl ester (60 mg, 0.27 mmol), (3-chloro-2-fluoro-phenyl)-hydrazine (Apollo Scientific, Ltd., 54 mg, 0.27 mmol), and zinc chloride (110 mg, 0.8 mmol) in acetic acid (2 mL) is purged with nitrogen for 5 minutes and then heated in a sealed tube at 120° C. for 2 hours. The mixture is cooled to room temperature and diluted with ethyl acetate. The resulting mixture is sequentially washed with saturated aqueous Na2CO3 and saturated aqueous NaCl, and finally dried over sodium sulfate. After concentration, the crude product is purified via silica gel flash column chromatography (10% ethyl acetate in hexanes) to afford 4-(6-chloro-3-ethyl-7-fluoro-1H-indol-2-yl)-2-hydroxy-benzoic acid methyl ester as a light yellow solid: ESMS m/z 348.1 (M+H+). is purged with nitrogen for 5 minutes The mixture is cooled to room temperature diluted with ethyl acetate The resulting mixture is sequentially washed with saturated aqueous Na2CO3 and saturated aqueous NaCl finally dried over sodium sulfate After concentration the crude product is purified via silica gel flash column chromatography (10% ethyl acetate in hexanes)
来源 ID: ord-c96e38f34770433eaef37cda5194a561反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: The title compound, EI-MS: m/e=258.1 (M+), was prepared in accordance with the general method of example 25b) from (3-Chloro-2-fluoro-phenyl)-hydrazine and ethyl pyruvate.
来源 ID: ord-0a6950f5e4564622885e8b8ed23d9643反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-(3-trifluoromethansulfonyl-phenyl)-1H-pyridazin-4-one (A-33) and 3-chloro-2-fluoro-phenylhydrazine according to the method described for example 1. MS: M=499.0 (M+H)+ The product was obtained
来源 ID: ord-e09481eeffaf40c1835077646ffc58e7反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: The product was obtained starting from 3-((E)-3-Dimethylamino-acryloyl)-1-(4-trifluoromethansulfonyl-phenyl)-1H-pyridazin-4-one (A-27) and 3-chloro-2-fluoro-phenylhydrazine according to the method described for example 1. MS: M=499.0 (M+H)+ The product was obtained
来源 ID: ord-04247a6b206848948eaa32bb68a8bf3b反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: The title compound, EI-MS: m/e=258.1 (M+), was prepared in accordance with the general method of example 32d) from (3-Chloro-2-fluoro-phenyl)-hydrazine and ethyl pyruvate.
来源 ID: ord-12354a14485e420cac34010fd23c5db2反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: The title compound, EI-MS: m/e=258.1 (M+), was prepared in accordance with the general method of example 25b) from (3-Chloro-2-fluoro-phenyl)-hydrazine and ethyl pyruvate.
来源 ID: ord-fcdfbf94bd5a467d81576a3da1a93570PubChem References
以下资料来自该化合物的公开数据库参考记录。