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8 条反应 · 8 篇文献
反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-fd9fa37b0b224808909b9314a3634713反应条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: To a solution of 2,6-dimethyl aniline (50 gm) in 1,4-dioxane (400 ml) and pyridine (40 ml) was added iodine (157.3 gm) slowly at 0° C. The solution was stirred for 1 hour at 0° C. and the temperature was raised to room temperature. The solution was stirred for 1 hour at room temperature and then added a saturated solution of sodium thiosulfate. The layers were separated and the aqueous layer was extracted with methylene chloride. The combined organic layers were dried with anhydrous sodium sulfate and the solvent was evaporated in vacuum to obtain 91.8 gm of 4-iodo-2,6-dimethyl benzenamine. the temperature was raised to room temperature The solution was stirred for 1 hour at room temperature The layers were separated the aqueous layer was extracted with methylene chloride The combined organic layers were dried with anhydrous sodium sulfate the solvent was evaporated in vacuum
来源 ID: ord-394692fda96645f988ef30d8fef96a08反应条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: To a solution of 2,6-dimethyl aniline (50 gm) in 1,4-dioxane (400 ml) and pyridine (40 ml) was added iodine (157.3 gm) slowly at 0° C. The solution was stirred for 1 hour at 0° C. and the temperature was raised to room temperature. The solution was stirred for 1 hour at room temperature and then added a saturated solution of sodium thiosulfate. The layers were separated and the aqueous layer was extracted with methylene chloride. The combined organic layers were dried with anhydrous sodium sulfate and the solvent was evaporated in vacuum to obtain 91.8 gm of 4-iodo-2,6-dimethyl benzenamine. the temperature was raised to room temperature The solution was stirred for 1 hour at room temperature The layers were separated the aqueous layer was extracted with methylene chloride The combined organic layers were dried with anhydrous sodium sulfate the solvent was evaporated in vacuum
来源 ID: ord-394692fda96645f988ef30d8fef96a08反应条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: To a solution of 2,6-dimethyl aniline (25 gm) in 1,4-dioxane (200 ml) and dimethylacetamide (20 ml) was added iodine (79 gm) slowly at 0° C. The solution was stirred for 1 hour at 0° C. and the temperature was raised to room temperature. The solution was stirred for 1 hour at room temperature and then added a saturated solution of sodium thiosulfate. The layers were separated and the aqueous layer was extracted with methylene chloride. The combined organic layers were dried with anhydrous sodium sulfate and the solvent was evaporated in vacuum to obtain 45 gm of 4-iodo-2,6-dimethyl benzenamine. the temperature was raised to room temperature The solution was stirred for 1 hour at room temperature The layers were separated the aqueous layer was extracted with methylene chloride The combined organic layers were dried with anhydrous sodium sulfate the solvent was evaporated in vacuum
来源 ID: ord-cb9305547de8470f988989b2f585f61f反应条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: To a solution of 2,6-dimethyl aniline (50 gm) in 1,4-dioxane (400 ml) and N-methylpyrrolidone (40 ml) was added iodine (157.3 gm) slowly at 0° C. The solution was stirred for 1 hour at 0° C. and the temperature was raised to room temperature. The solution was stirred for 1 hour at room temperature and then added a saturated solution of sodium thiosulfate. The layers were separated and the aqueous layer was extracted with methylene chloride. The combined organic layers were dried with anhydrous sodium sulfate and the solvent was evaporated in vacuum to obtain 91 gm of 4-iodo-2,6-dimethyl benzenamine. the temperature was raised to room temperature The solution was stirred for 1 hour at room temperature The layers were separated the aqueous layer was extracted with methylene chloride The combined organic layers were dried with anhydrous sodium sulfate the solvent was evaporated in vacuum
来源 ID: ord-5407fc16acc14e34a5f9995983dc505a反应条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: To a solution of 2,6-dimethyl aniline (50 gm) in 1,4-dioxane (400 ml) and pyridine (40 ml) was added iodine (157.3 gm) slowly at 0° C. The solution was stirred for 1 hour at 0° C. and the temperature was raised to room temperature. The solution was stirred for 1 hour at room temperature and then added a saturated solution of sodium thiosulfate. The layers were separated and the aqueous layer was extracted with methylene chloride. The combined organic layers were dried with anhydrous sodium sulfate and the solvent was evaporated in vacuum to obtain 91.8 gm of 4-iodo-2,6-dimethyl benzenamine. the temperature was raised to room temperature The solution was stirred for 1 hour at room temperature The layers were separated the aqueous layer was extracted with methylene chloride The combined organic layers were dried with anhydrous sodium sulfate the solvent was evaporated in vacuum
来源 ID: ord-d5508c13a42645a7b39165f3954ffde6反应条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: To a solution of 2,6-dimethyl aniline (50 gm) in 1,4-dioxane (400 ml) and pyridine (40 ml) was added iodine (157.3 gm) slowly at 0° C. The solution was stirred for 1 hour at 0° C. and the temperature was raised to room temperature. The solution was stirred for 1 hour at room temperature and then added a saturated solution of sodium thiosulfate. The layers were separated and the aqueous layer was extracted with methylene chloride. The combined organic layers were dried with anhydrous sodium sulfate and the solvent was evaporated in vacuum to obtain 91.8 gm of 4-iodo-2,6-dimethyl benzenamine. the temperature was raised to room temperature The solution was stirred for 1 hour at room temperature The layers were separated the aqueous layer was extracted with methylene chloride The combined organic layers were dried with anhydrous sodium sulfate the solvent was evaporated in vacuum
来源 ID: ord-d5508c13a42645a7b39165f3954ffde6反应条件: temp:0.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: To a solution of 2,6-dimethyl aniline (50 gm) in 1,4-dioxane (400 ml) and pyridine (40 ml) was added iodine (157.3 gm) slowly at 0° C. The solution was stirred for 1 hour at 0° C. and the temperature was raised to room temperature. The solution was stirred for 1 hour at room temperature and then added a saturated solution of sodium thiosulfate. The layers were separated and the aqueous layer was extracted with methylene chloride. The combined organic layers were dried with anhydrous sodium sulfate and the solvent was evaporated in vacuum to obtain 91.8 gm of 4-iodo-2,6-dimethyl benzenamine. the temperature was raised to room temperature The solution was stirred for 1 hour at room temperature The layers were separated the aqueous layer was extracted with methylene chloride The combined organic layers were dried with anhydrous sodium sulfate the solvent was evaporated in vacuum
来源 ID: ord-394692fda96645f988ef30d8fef96a08PubChem References
以下资料来自该化合物的公开数据库参考记录。