2,4,6-三甲基苯硼酸

反应条件: temp:0.00; pressure:0.00; stir:

反应条件: temp:0.00; pressure:0.00; stir:

反应条件: temp:0.00; pressure:0.00; stir:

反应条件: temp:0.00; pressure:0.00; stir:

反应条件: temp:0.00; pressure:0.00; stir:

反应条件: temp:0.00; pressure:0.00; stir:

反应条件: temp:60.01; pressure:0.00; stir:

实验步骤: pre-ligate Ni(cod)2 and phosphine ligand in dioxane for 15 minutes in a separate plate Dilute with acetonitrile Diluent solution was made in 1 L batches with 950 mL acetonitrile, 25 mL water, 25 mL glacial acetic acid, and 53 mg 4,4’-di-tert-butylbiphenyl as an external standard (0.2 equiv standard per reaction). Aliquot taken from each well (47 ul) is added into 753 ul of diluent solution

反应条件: temp:60.01; pressure:0.00; stir:

实验步骤: pre-ligate Ni(cod)2 and phosphine ligand in dioxane for 15 minutes in a separate plate Dilute with acetonitrile Diluent solution was made in 1 L batches with 950 mL acetonitrile, 25 mL water, 25 mL glacial acetic acid, and 53 mg 4,4’-di-tert-butylbiphenyl as an external standard (0.2 equiv standard per reaction). Aliquot taken from each well (47 ul) is added into 753 ul of diluent solution

反应条件: temp:60.01; pressure:0.00; stir:

实验步骤: pre-ligate Ni(cod)2 and phosphine ligand in dioxane for 15 minutes in a separate plate Dilute with acetonitrile Diluent solution was made in 1 L batches with 950 mL acetonitrile, 25 mL water, 25 mL glacial acetic acid, and 53 mg 4,4’-di-tert-butylbiphenyl as an external standard (0.2 equiv standard per reaction). Aliquot taken from each well (47 ul) is added into 753 ul of diluent solution

反应条件: temp:60.01; pressure:0.00; stir:

实验步骤: pre-ligate Ni(cod)2 and phosphine ligand in dioxane for 15 minutes in a separate plate Dilute with acetonitrile Diluent solution was made in 1 L batches with 950 mL acetonitrile, 25 mL water, 25 mL glacial acetic acid, and 53 mg 4,4’-di-tert-butylbiphenyl as an external standard (0.2 equiv standard per reaction). Aliquot taken from each well (47 ul) is added into 753 ul of diluent solution

反应条件: temp:60.01; pressure:0.00; stir:

实验步骤: pre-ligate Ni(cod)2 and phosphine ligand in dioxane for 15 minutes in a separate plate Dilute with acetonitrile Diluent solution was made in 1 L batches with 950 mL acetonitrile, 25 mL water, 25 mL glacial acetic acid, and 53 mg 4,4’-di-tert-butylbiphenyl as an external standard (0.2 equiv standard per reaction). Aliquot taken from each well (47 ul) is added into 753 ul of diluent solution

反应条件: temp:60.01; pressure:0.00; stir:

实验步骤: pre-ligate Ni(cod)2 and phosphine ligand in dioxane for 15 minutes in a separate plate Dilute with acetonitrile Diluent solution was made in 1 L batches with 950 mL acetonitrile, 25 mL water, 25 mL glacial acetic acid, and 53 mg 4,4’-di-tert-butylbiphenyl as an external standard (0.2 equiv standard per reaction). Aliquot taken from each well (47 ul) is added into 753 ul of diluent solution