卤丙烷

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: The general procedure of Example 56 was repeated using 4-n-pentenyl-4-phenyl-4-silacyclohexane carbaldehyde, 4-(t-butyldimethylsiloxy)benzyltriphenylphosphonium bromide, and 1-bromo-2,2,3,3-tetrafluoropropane, thereby obtaining the intended compound. obtaining the intended compound

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: The general procedure of Example 56 was repeated using 4-n-pentenyl-4-phenyl-4-silacyclohexane carbaldehyde, 4-(t-butyldimethylsiloxy)benzyltriphenylphosphonium bromide, and 1-bromo-2,2,3,3-tetrafluoropropane, thereby obtaining the intended compound. obtaining the intended compound

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: The general procedure of Example 17 was repeated using 4'-bromo-4-(t-butyldimethylsiloxy)biphenyl, 4-pentyl-4-phenyl-4-silacyclohexanone, and 1-bromo-2,2,3,3-tetrafluoro-n-propane, thereby obtaining the intended compound. obtaining the intended compound

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: The general procedure of Example 17 was repeated using 4'-bromo-3-fluoro-4-(t-butyldimethylsiloxy)biphenyl, 4-pentyl-4-phenyl-4-silacyclohexanone, and 1-bromo-2,2,3,3-tetrafluoro-n-propane, thereby obtaining the intended compound. obtaining the intended compound

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: The general procedure of Example 17 was repeated using 4'-bromo-3-fluoro-4-(t-butyldimethylsiloxy)biphenyl, 4-pentyl-4-phenyl-4-silacyclohexanone, and 1-bromo-2,2,3,3-tetrafluoro-n-propane, thereby obtaining the intended compound. obtaining the intended compound

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: The general procedure of Example 56 was repeated using 4-n-pentenyl-4-phenyl-4-silacyclohexane carbaldehyde, 4-(t-butyldimethylsiloxy)benzyltriphenylphosphonium bromide, and 1-bromo-2,2,3,3-tetrafluoropropane, thereby obtaining the intended compound. obtaining the intended compound

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: The general procedure of Example 17 was repeated using 4'-bromo-4-(t-butyldimethylsiloxy)biphenyl, 4-pentyl-4-phenyl-4-silacyclohexanone, and 1-bromo-2,2,3,3-tetrafluoro-n-propane, thereby obtaining the intended compound. obtaining the intended compound

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: The general procedure of Example 17 was repeated using 4'-bromo-3-fluoro-4-(t-butyldimethylsiloxy)biphenyl, 4-pentyl-4-phenyl-4-silacyclohexanone, and 1-bromo-2,2,3,3-tetrafluoro-n-propane, thereby obtaining the intended compound. obtaining the intended compound