反应 #3868169
相关文献 (1)
openreactiondata ↗doi:10.1039/C8SC04228D
反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-c018697ff57747e7ba6e7f2915da0343暂无可渲染的结构数据
CC(C)CCCCCCCCCCO产品信息
C11-14-异构醇(主要为C13-醇)(CAS 68526-86-3)的产品身份、结构标识及相关反应资料,供化学中间体检索、研发和采购评估使用。
可能的应用方向
仅供专业研发与工业用途
数据库编号 33865
安全提示
仅供专业研发与工业用途。操作前请依据供应商提供的安全数据表完成风险评估。
合成路线数据
10 条反应 · 10 篇文献
反应条件: temp:0.00; pressure:0.00; stir:
来源 ID: ord-c018697ff57747e7ba6e7f2915da0343反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: Preparation according to Example 3 from 3,5,5-trimethyl-hexanoic acid and isotridecyl alcohol (mixture of methyl branched primary tridecanols from Hoechst); colorless liquid of medium viscosity; Preparation
来源 ID: ord-8ced3bcd008e4204adab28dd800f78fb反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: Preparation according to Example 3 from 3,5,5-trimethyl-hexanoic acid and isotridecyl alcohol (mixture of methyl branched primary tridecanols from Hoechst); colorless liquid of medium viscosity; Preparation
来源 ID: ord-8ced3bcd008e4204adab28dd800f78fb反应条件: temp:340.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 180 kg of isotridecyl alcohol and 33.6 kg of NaOH were introduced into the 350 liter reactor and heated to 340° C. under a nitrogen pressure of 6 bar. The process was otherwise carried out as described in Example 1. The product obtained had an acid value of 240 and an OH value of 6.3. The product obtained
来源 ID: ord-f441da02fbca4202b1a3755c32f10e74反应条件: temp:340.01; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 180 kg of isotridecyl alcohol and 33.6 kg of NaOH were introduced into the 350 liter reactor and heated to 340° C. under a nitrogen pressure of 6 bar. The process was otherwise carried out as described in Example 1. The product obtained had an acid value of 240 and an OH value of 6.3. The product obtained
来源 ID: ord-f441da02fbca4202b1a3755c32f10e74反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: This compound was prepared from 4-hydroxybenzoic acid methylester and isotridecylchloride, initially obtained from isotridecanol (an oxalcohol prepared from tetrapropylene) using known techniques. The product recovered exhibited a refractive index of
来源 ID: ord-042c2ac25241438a9cc4967aa8083194反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: The sebocyte assay procedure described in Example 2 was repeated with additional branched esters. The results that were obtained are summarized in Table 4. Isotridecyl linoleate and isotridecyl benzoate were synthesised according to the procedure of Example 1, using Exxal® 13 isotridecanol as starting material. The results that were obtained are summarized in Table 5. Phenol Red was used as a positive control. The results that were obtained The results that were obtained
来源 ID: ord-05f803e6aa034628bca47ea8ec98f0cf反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: A process for the preparation of solid active-ingredient concentrates, which comprises preparing a spray solution from sodium cumenesulphonate, methylhydroxyethylcellulose and water which is sprayed onto a mixture of magnesium perphthalate powder and sodium alkylbenzoate powder in a fluidized-bed drier at an air intake temperature of from about 60 to 80° C., and coating the granules formed with a melt of isotridecanol ethoxylate. A process for the preparation of solid active-ingredient concentrates, which
来源 ID: ord-53da5a1ad08542989544f728e16dd5e5反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: 7.13 g (20 mmol) of 1,2,3,4,5-pentamethoxycarbonylcyclopentadiene are treated with 20.0 g (100 mmol) of isotridecyl alcohol. 3.12 g (97.5% of the theoretical yield) of methanol are distilled off at 100° C. within 8 h, firstly at 1013 mbar, then at from 363 to 18 mbar. 24 g of 1,2,3,4,5-pentaisotridecyloxycarbonylcyclopentadiene are obtained. are distilled off at 100° C. within 8 h, firstly at 1013 mbar
来源 ID: ord-06999c9c110c4195ad4f0e20ffd54137反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.
实验步骤: Preparation according to Example 3 from 3,5,5-trimethyl-hexanoic acid and isotridecyl alcohol (mixture of methyl branched primary tridecanols from Hoechst); colorless liquid of medium viscosity; Preparation
来源 ID: ord-8ced3bcd008e4204adab28dd800f78fbPubChem References
以下资料来自该化合物的公开数据库参考记录。
相关产品
12 related records
CAS 20194-45-0
CAS 90200-61-6
CAS 2370-13-0
CAS 72890-46-1
CAS 54322-29-1
CAS 38514-02-2
CAS 6345-85-3
CAS 5333-42-6
CAS 2938-98-9
CAS 32444-34-1
CAS 4448-75-3
CAS 55505-28-7
