2,2-二甲基丙基 乙酸甲酯

反应条件: temp:0.00; pressure:0.00; stir:

反应条件: temp:0.00; pressure:0.00; stir:

反应条件: temp:75.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: 6.47 g (82.5 mmol) of acetyl chloride were added dropwise with stirring at 20° C. to a solution of 6.61 g (75.0 mmol) of neopentyl alcohol (2,2-dimethyl-1-propanol) and 6.76 g (82.5 mmol) of 1-methylimidazole. The reaction mixture was stirred for a further 30 min and then heated to 75° C. The suspension which had formed in the meantime was converted to a liquid biphasic mixture. Removal of the upper phase gave 8.40 g (theory: 9.76 g) of neopentyl acetate as a colorless oil having a purity of 98% (GC). The suspension which had formed in the meantime Removal of the upper phase

反应条件: temp:20.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: 6.47 g (82.5 mmol) of acetyl chloride were added dropwise to a solution of 6.61 g (75.0 mmol) of neopentyl alcohol (2,2-dimethyl-1-propanol) and 6.76 g (82.5 mmol) of 1-methylimidazole while stirring at 20° C. The reaction mixture was stirred for a further 30 minutes and subsequently heated to 75° C. This resulted in the suspension initially formed being converted into a liquid two-phase mixture. The upper phase was separated off to give 8.40 g (theory: 9.76 g) of neopentyl acetate as a colorless oil having a purity of 98% (GC). The reaction mixture was stirred for a further 30 minutes subsequently heated to 75° C This resulted in the suspension initially formed The upper phase was separated off

反应条件: temp:20.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: 6.47 g (82.5 mmol) of acetyl chloride were added dropwise to a solution of 6.61 g (75.0 mmol) of neopentyl alcohol (2,2-dimethyl-1-propanol) and 6.76 g (82.5 mmol) of 1-methylimidazole while stirring at 20° C. The reaction mixture was stirred for a further 30 minutes and subsequently heated to 75° C. This resulted in the suspension initially formed being converted into a liquid two-phase mixture. The upper phase was separated off to give 8.40 g (theory: 9.76 g) of neopentyl acetate as a colorless oil having a purity of 98% (GC). The reaction mixture was stirred for a further 30 minutes subsequently heated to 75° C This resulted in the suspension initially formed The upper phase was separated off

反应条件: temp:75.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: 6.47 g (82.5 mmol) of acetyl chloride were added dropwise with stirring at 20° C. to a solution of 6.61 g (75.0 mmol) of neopentyl alcohol (2,2-dimethyl-1-propanol) and 6.76 g (82.5 mmol) of 1-methylimidazole. The reaction mixture was stirred for a further 30 min and then heated to 75° C. The suspension which had formed in the meantime was converted to a liquid biphasic mixture. Removal of the upper phase gave 8.40 g (theory: 9.76 g) of neopentyl acetate as a colorless oil having a purity of 98% (GC). The suspension which had formed in the meantime Removal of the upper phase

反应条件: temp:20.01; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: 6.47 g (82.5 mmol) of acetyl chloride were added dropwise to a solution of 6.61 g (75.0 mmol) of neopentyl alcohol (2,2-dimethyl-1-propanol) and 6.76 g (82.5 mmol) of 1-methylimidazole while stirring at 20° C. The reaction mixture was stirred for a further 30 minutes and subsequently heated to 75° C. This resulted in the suspension initially formed being converted into a liquid two-phase mixture. The upper phase was separated off to give 8.40 g (theory: 9.76 g) of neopentyl acetate as a colorless oil having a purity of 98% (GC). The reaction mixture was stirred for a further 30 minutes subsequently heated to 75° C This resulted in the suspension initially formed The upper phase was separated off