四甲基碘化磷

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Cyclotetradecene (4.0 g), chloroform (18 ml), 50% aqueous sodium hydroxide solution (22 ml), dichloromethane (5 ml), n-octane (1 ml) and tetramethylphosphonium iodide (0.01 g) were stirred together at 35° C. for 3 hours. At the end of this period the conversion of starting material to the desired product was found by GLC to be 100%.

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Cyclotetradecene (4.0 g), chloroform (18 ml), 50% aqueous sodium hydroxide solution (22 ml), dichloromethane (5 ml), n-octane (1 ml) and tetramethylphosphonium iodide (0.01 g) were stirred together at 35° C. for 3 hours. At the end of this period the conversion of starting material to the desired product was found by GLC to be 100%.

反应条件: temp:0.00; pressure:0.00; stir:; See reaction.notes.procedure_details.

实验步骤: Cyclotetradecene (4.0 g), chloroform (18 ml), 50% aqueous sodium hydroxide solution (22 ml), dichloromethane (5 ml), n-octane (1 ml) and tetramethylphosphonium iodide (0.01 g) were stirred together at 35° C. for 3 hours. At the end of this period the conversion of starting material to the desired product was found by GLC to be 100%.